Simultaneous determination of ten aminoglycoside antibiotics in aquatic feeds by high-performance liquid chromatography quadrupole-orbitrap mass spectrometry with pass-through cleanup
文献类型： 外文期刊
作者： Lou, Xiaoyi 1 ; Tang, Yunyu 1 ; Fang, Changling 1 ; Kong, Cong 1 ; Yu, Huijuan 1 ; Shi, Yongfu 1 ; Huang, Dongmei 1 ; Guo 1 ;
作者机构： 1.Chinese Acad Fishery Sci, East China Sea Fisheries Res Inst, Lab Qual Safety & Proc Aquat Prod, Shanghai, Peoples R China
2.Minist Agr & Rural Affairs, Key Lab Control Qual & Safety Aquat Prod, Beijing, Peoples R China
3.Shanghai Polytech Univ, Res Ctr Resource Recycling Sci & Engn, Sch Environm & Mat Engn, Shanghai, Peoples R China
4.City Univ Hong Kong, Dept Phys, Hong Kong, Peoples R China
5.Fudan Univ, Dept Environm Sci & Engn, Shanghai, Peoples R China
关键词： antibiotic residues; exploration of detection method; instrumental analysis; modified solid phase extraction; optimization
期刊名称：CHIRALITY （ 影响因子：2.437； 五年影响因子：2.204 ）
ISSN： 0899-0042
年卷期： 2020 年 32 卷 3 期
页码：
收录情况： SCI
摘要： A simple and sensitive method has been established based on pass-through cleanup and high-performance liquid chromatography quadrupole-orbitrap mass spectrometry (HPLC-Q/Orbitrap MS) for the simultaneous determination of ten aminoglycosides (AGs) in aquatic feeds. The extraction solution and cleanup procedure had been optimized, and good sensitivity, accuracy, and precision were obtained. The calibration curves of AGs were linearity (R-2 > 0.99) in the range of 2.0 to 200 mu g/L (or 5.0 to 500 mu g/L). The limits of detection of AGs were between 10 and 25 mu g/kg. The recoveries of AGs ranged from 74.9% to 94.3%, and the intraday and interday relative standard deviations were less than 15%. Finally, this method was successfully applied to determine ten AGs in 30 aquatic feed samples. It might be the first time to use pass-through cleanup approach combined with HPLC-Q/Orbitrap MS method for AGs determination in aquatic feed samples.
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