Simultaneous Determination of Five Benzimidazoles in Feeds Using High-Performance Capillary Electrophoresis
文献类型： 外文期刊
作者： Shen, Jianzhong 1 ; Tong, Jing 1 ; Jiang, Haiyang 1 ; Rao, Qinxiong 2 ; Li, Na 1 ; Guo, Liming 1 ; Ding, Shuangyang 1 ;
作者机构： 1.China Agr Univ, Natl Reference Labs Vet Drug Residue, Dept Vet Pharmacol & Toxicol, Coll Vet Med, Beijing 100193, Peoples R China
2.Shanghai Acad Agr Sci, Inst Agrofood Stand & Testing, Shanghai 201106, Peoples R China
关键词： animal feed;poultry feed;swine feed
期刊名称：JOURNAL OF AOAC INTERNATIONAL （ 影响因子：1.913； 五年影响因子：1.754 ）
ISSN：
年卷期：
页码：
收录情况： SCI
摘要： A high-performance capillary electrophoretic method for determination of five benzimidazoles (thiabendazole, albendazole, fenbendazole, mebendazole, oxfendazole) in animal feeds was developed. Separation was carried out in an 80.5 cm x 75 mu m id fused-silica uncoated capillary and injected by hydrodynamic injection (35 mbar x 8 s) at a wavelength detection of 295 nm. The drugs were completely resolved in 50 mmol/L citric acid buffer (pH 1.9) with 30 W at a temperature of 25 degrees C. Linear range was 1-80 mu g/mL; limits of detection for the analytes were less than 2 mg/kg; the overall recoveries for benzimidazoles were >73%, with coefficients of variation below 10%.
- 相关文献
作者其他论文 更多>>
-
Isotope Ratio Mass Spectrometry (IRMS)-Based Authentication of the Geographic Origins of Volvariella volvacea (Bull.) Singer
作者：Liu, Xing;Liu, Zhu;Li, Peijun;Liu, Xing;Rao, Qinxiong;Zhang, Qicai;Geng, Hao;Lu, Yangyang;Chen, Shanshan;Song, Weiguo;Liu, Xing;Rao, Qinxiong;Zhang, Qicai;Geng, Hao;Lu, Yangyang;Chen, Shanshan;Song, Weiguo;Liu, Zhu;Li, Peijun
关键词：
Volvariella volvacea ; stable isotope; nutrition component; geographic origin; PLS-DA -
Non-targeted metabolomics studies revealed the effects of environmentally relevant concentrations of perfluorooctane sulfonic acid (PFOS) on carbohydrate metabolism in red claw crayfish (Cherax quadricarinatus)
作者：Hong, Shuang;Liu, Chengbin;Liu, Xiaoyu;Rao, Qinxiong;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Song, Weiguo;Hong, Shuang
关键词：Perfluoroctane sulfonate; Environmental relevant concentration; Cherax quadricarinatus; Metabolomics; Carbohydrate metabolism
-
Multivariate fusion for identification of geographic origins and varieties of coix seed
作者：Liu, Xing;Fan, Kai;Lu, Yangyang;Rao, Qinxiong;Zhang, Qicai;Geng, Hao;Song, Weiguo;Liu, Xing;Fan, Kai;Lu, Yangyang;Rao, Qinxiong;Zhang, Qicai;Geng, Hao;Song, Weiguo;Wang, Zhengwu
关键词：
-
Neurodevelopmental effects of exposure to environmentally relevant concentrations of perfluorooctane sulfonic acid (PFOS), perfluorobutanesulfonic acid (PFBS) and 6:2 chlorinated polyfluorinated ether sulfonate (6:2 Cl-PFESA) on larval zebrafish: Multi-omics and neuropathology perspective
作者：Cao, Xiaolong;Chen, Haolei;Cao, Xiaolong;Li, Yameng;Liu, Xiaoyu;Li, Kepiao;Hong, Shuang;Chen, Haolei;Rao, Qinxiong;Li, Huaxi;Deng, Zhongsheng;Song, Weiguo;Li, Yameng;Liu, Xiaoyu;Li, Kepiao;Hong, Shuang;Rao, Qinxiong;Li, Huaxi;Deng, Zhongsheng;Song, Weiguo;Li, Huaxi;Deng, Zhongsheng;Song, Weiguo
关键词：PFOS and its substitutes; Zebrafish; Environmentally relevant concentrations; Multi-omics analysis; Neurodevelopmental effects
-
Origin Traceability of Chinese Mitten Crab (Eriocheir sinensis) Using Multi-Stable Isotopes and Explainable Machine Learning
作者：Wang, Danhe;Yao, Chunxia;Lu, Yangyang;Huang, Di;Li, Yameng;Song, Weiguo;Wang, Danhe;Yao, Chunxia;Lu, Yangyang;Huang, Di;Li, Yameng;Song, Weiguo;Wu, Xugan;Rao, Qinxiong
关键词：Chinese mitten crab; origin traceability; stable isotopes; explainable machine learning; tissue specificity
-
Assessing Seasonal Effects on Identification of Cultivation Methods of Short-Growth Cycle Brassica chinensis L. Using IRMS and NIRS
作者：Liu, Xing;Fan, Kai;Lu, Yangyang;Zhao, Hong;Rao, Qinxiong;Geng, Hao;Chen, Yijiao;Song, Weiguo;Liu, Xing;Fan, Kai;Lu, Yangyang;Zhao, Hong;Rao, Qinxiong;Geng, Hao;Chen, Yijiao;Song, Weiguo;Rogers, Karyne Maree;Rogers, Karyne Maree
关键词：Brassica chinensis L.; seasonal effect; stable isotope; NIRS; cultivation method; PLS-DA
-
A novel, low-cost, and efficient separation strategy based on S-doped C3N4 for the analysis of PCDD/Fs and dioxin-like PCBs
作者：Luo, Yanli;Luo, Yanli;Liu, Chengbin;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Huang, Di;Liu, Xing;Lu, Yangyang;Song, Wei;Chen, Shanshan;Zhou, Jiaxin;Rao, Qinxiong;Song, Weiguo;Liu, Chengbin;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Huang, Di;Liu, Xing;Lu, Yangyang;Song, Wei;Chen, Shanshan;Zhou, Jiaxin;Rao, Qinxiong;Liu, Chengbin;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Huang, Di;Liu, Xing;Lu, Yangyang;Song, Wei;Chen, Shanshan;Zhou, Jiaxin;Rao, Qinxiong
关键词：PCDD/Fs; Dl-PCBs; Carbon nitride; Separation; Analysis
