Simultaneous determination of five tetracycline and macrolide antibiotics in feeds using HPCE
文献类型： 外文期刊
作者： Tong, Jing 1 ; Rao, Qinxiong 2 ; Zhu, Kui 1 ; Jiang, Zhigang 1 ; Ding, Shuangyang 1 ;
作者机构： 1.China Agr Univ, Coll Vet Med, Dept Pharmacol & Toxicol, Beijing 100094, Peoples R China
2.Shanghai Acad Agr Sci, Inst Agrofood Stand & Testing, Shanghai, Peoples R China
关键词： Animal feeds;HPCE;Macrolide antibiotics;Tetracycline antibiotics
期刊名称：JOURNAL OF SEPARATION SCIENCE （ 影响因子：3.645； 五年影响因子：2.943 ）
ISSN：
年卷期：
页码：
收录情况： SCI
摘要： This work demonstrates the potential of HPCE in the analysis of antibiotics in a complex matrix such as feedstuffs. Using 20 mM citric acid-40 mM Na2HPO4 buffer (pH 2.65), the five antibiotics, tetracycline, oxytetracycline, doxycycline, tilmicosin, and tylosin were successfully separated at 30 kV in a 64.5 cm x 75 pm. id capillary. Good repeatability, stability, and reliability of the method were supported by < 10% CV with mean recoveries of > 70%, and the limit of detection of the five analytes was 0.5-1 mg/kg. It was for the first time that a capillary electrophoretic method was employed to simultaneously detect five tetracycline and macrolide antibiotics in animal feeds.
- 相关文献
作者其他论文 更多>>
-
Assessing Seasonal Effects on Identification of Cultivation Methods of Short-Growth Cycle Brassica chinensis L. Using IRMS and NIRS
作者：Liu, Xing;Fan, Kai;Lu, Yangyang;Zhao, Hong;Rao, Qinxiong;Geng, Hao;Chen, Yijiao;Song, Weiguo;Liu, Xing;Fan, Kai;Lu, Yangyang;Zhao, Hong;Rao, Qinxiong;Geng, Hao;Chen, Yijiao;Song, Weiguo;Rogers, Karyne Maree;Rogers, Karyne Maree
关键词：Brassica chinensis L.; seasonal effect; stable isotope; NIRS; cultivation method; PLS-DA
-
A novel, low-cost, and efficient separation strategy based on S-doped C3N4 for the analysis of PCDD/Fs and dioxin-like PCBs
作者：Luo, Yanli;Luo, Yanli;Liu, Chengbin;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Huang, Di;Liu, Xing;Lu, Yangyang;Song, Wei;Chen, Shanshan;Zhou, Jiaxin;Rao, Qinxiong;Song, Weiguo;Liu, Chengbin;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Huang, Di;Liu, Xing;Lu, Yangyang;Song, Wei;Chen, Shanshan;Zhou, Jiaxin;Rao, Qinxiong;Liu, Chengbin;Wang, Xianli;Zhang, Qicai;Yao, Chunxia;Huang, Di;Liu, Xing;Lu, Yangyang;Song, Wei;Chen, Shanshan;Zhou, Jiaxin;Rao, Qinxiong
关键词：PCDD/Fs; Dl-PCBs; Carbon nitride; Separation; Analysis
-
Exploring a novel, sensitive, and efficient Pb2+electrochemical sensing strategy based on Cu-MOF
作者：Yao, Chunxia;Wang, Hongmei;Zhou, Jiaxin;Song, Wei;Rao, Qinxiong;Liu, Chengbin;Song, Weiguo;Yao, Chunxia;Zhou, Jiaxin;Song, Wei;Rao, Qinxiong;Liu, Chengbin;Song, Weiguo;Yao, Chunxia;Zhou, Jiaxin;Song, Wei;Rao, Qinxiong;Liu, Chengbin;Song, Weiguo;Wang, Hongmei;Gao, Zhaoliang;Liang, Ying
关键词：MOFs; Electrochemical sensor; Environmental analysis; Heavy metals; Lead; Dissolution voltammetry
-
Tissue distribution and exposure risk assessment of dioxins, dioxin-like polychlorinated biphenyls and perfluoroalkyl substances in red swamp crayfish
作者：Wang, Xianli;Rao, Qinxiong;Zhang, Qicai;Liu, Chengbin;Li, Yameng;Wang, Danhe;Huang, Di;Yao, Chunxia;Song, Weiguo;Li, Yanshen;Wang, Xianli;Rao, Qinxiong;Zhang, Qicai;Liu, Chengbin;Li, Yameng;Wang, Danhe;Huang, Di;Yao, Chunxia;Song, Weiguo
关键词：Red swamp crayfish; Persistent organic pollutants; Tissue distribution; Health risk
-
Determination of 25 polybrominated diphenyl ethers in Chinese mitten crab ecosystems by gas chromatography-mass spectrometry
作者：Zhang, Qicai;Song, Weiguo;Wang, Xianli;Liu, Chengbin;Chen, Shanshan;Li, Huaxi;Rao, Qinxiong;Zhang, Qicai;Song, Weiguo;Wang, Xianli;Liu, Chengbin;Chen, Shanshan;Li, Huaxi;Rao, Qinxiong
关键词：
-
Hepatotoxicity evaluation and possible mechanisms of decabrominated diphenyl ethers (BDE-209) in broilers: Oxidative stress, inflammatory, and transcriptomics
作者：Yang, Yi;Rao, Qinxiong;Zhao, Zhihui;Yang, Junhua;Jin, Yuhong;Zhu, Xing
关键词：BDE-209; Hepatotoxicity; Oxidative stress; Inflammation; Transcriptomics
-
Effects of Thiamethoxam and Fenvalerate Residue Levels on Light-Stable Isotopes of Leafy Vegetables
作者：Qi, Fang;Liu, Xing;Deng, Zhongsheng;Lu, Yangyang;Chen, Yijiao;Geng, Hao;Zhang, Qicai;Rao, Qinxiong;Song, Weiguo;Qi, Fang;Liu, Xing;Deng, Zhongsheng;Lu, Yangyang;Chen, Yijiao;Geng, Hao;Zhang, Qicai;Rao, Qinxiong;Song, Weiguo
关键词：thiamethoxam; fenvalerate; spinach; cabbage; lettuce; light-stable isotopes; relationship; PLS-DA
