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Dissipation and safety evaluation of novaluron, pyriproxyfen, thiacloprid and tolfenpyrad residues in the citrus-field ecosystem

文献类型： 外文期刊

作者： Dong, Maofeng 1 ; Wen, Guangyue 1 ; Tang, Hongxia 1 ; Wang, Tan 1 ; Zhao, Zhihui 1 ; Song, Weiguo 1 ; Wang, Weimin 1 ; Zh 1 ;

作者机构： 1.Shanghai Acad Agr Sci, Pesticide Safety Evaluat Res Ctr, Inst Agrofood Stand & Testing Technol, Shanghai 2011106, Peoples R China

2.Shanghai Agr Tech Extens Serv Ctr, Shanghai 201103, Peoples R China

关键词： Citrus; Safety evaluation; Novaluron; Pyriproxyfen; Thiacloprid; Tolfenpyrad

期刊名称：FOOD CHEMISTRY （ 影响因子：7.514； 五年影响因子：7.516 ）

ISSN： 0308-8146

年卷期： 2018 年 269 卷

页码：

收录情况： SCI

摘要： The dissipations and residues of four pesticides in citrus, under field conditions, were measured using solid-phase extraction and LC-MS/MS. In the method validation, satisfactory results were obtained with fortified recoveries ranging from 80.6 to 113% and relative standard deviations <= 9.0%. In the dissipation test, the half-lives for the pesticides in citrus, according to first-order kinetics, ranged from 13.3 to 28.9 days. Based on the terminal residue test, two evaluation models (hazard quotient, HQ; risk quotient, RQ) were applied on citrus fruits for dietary exposure risk assessment. The results showed that HQs ranged from 0.0031 to 0.78%, and RQs from 7.3 to 57%, which are both acceptable for human consumption. Therefore, 14-day was proposed as a pre-harvest interval for the target compounds in citrus fruits. This work also contributes to residue data and, therefore, scientifically validated maximum residue limits in citrus, which are lacking in China currently.

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