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A fast and sensitive ultra-high-performance liquid chromatography-tandem mass spectrometry method for determining mefentrifluconazole in plant- and animal-derived foods

文献类型： 外文期刊

作者： Zhang, Ying 1 ; Wu, Xiaohu 1 ; Li, Xianbin 3 ; Duan, Tingting 2 ; Xu, Jun 1 ; Dong, Fengshou 1 ; Liu, Xingang 1 ; Guo, Lu 1 ;

作者机构： 1.Chinese Acad Agr Sci, State Key Lab Biol Plant Dis & Int Pests, Key Lab Control Biol Hazard Factors Plant Origin, Inst Plant Protect,Minist Agr, Beijing, Peoples R China

2.Guizhou Acad Agr Sci, Inst Plant Protect, Guiyang, Guizhou, Peoples R China

3.Minist Agr & Rural Affairs, Inst Control Agrochem, Beijing, Peoples R China

关键词： Mefentrifluconazole; residue; plant-derived foods; animal-derived foods

期刊名称：FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT （ 影响因子：3.057； 五年影响因子：2.96 ）

ISSN： 1944-0049

年卷期：

页码：

收录情况： SCI

摘要： A rapid and sensitive ultra-high-performance liquid chromatography-tandem mass spectrometry method, in conjunction with multiwalled carbon nanotube purification, was developed to determine the mefentrifluconazole levels in grapes, cucumbers, tomatoes, peppers, wheat, maize, eggs, milk, pork, chicken, and fish. After purification, tandem mass spectrometry of mefentrifluconazole required <3.0 min. Matrix-matched external standard curves were used to quantify the residual mefentrifluconazole. The method meets the requirements of the European Union Document SANTE/11813/2017. Quantification was linear between 5 and 500 mu g/kg (R-2 >= 0.9988), and both the intra- and interday relative standard deviations were <= 13.7%. Analyte recovery ranged from 81.5% to 107.6%. The limit of mefentrifluconazole quantification was 5 mu g/kg for all matrices. The method successfully detected and quantified mefentrifluconazole that had been applied to cucumbers and tomatoes grown in a test field. These results imply that the proposed method is effective and reliable for detecting mefentrifluconazole residues in plant- and animal-derived foods.

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