Novel carrier-mediated membrane-assisted three-phase liquid-liquid extraction coupled with liquid chromatography-mass spectrometry for the determination of eight biogenic amines in foods
文献类型： 外文期刊
作者： Zhou, Tian-Tian 1 ; Yigaimu, Aziguli 2 ; Muhammad, Turghun 1 ; Jian, Peng-Li 1 ; Sha, Li-Na 3 ; Zhang, Shu-Biao 4 ;
作者机构： 1.Xinjiang Univ, State Key Lab Chem & Utilizat Carbon Based Energy, Coll Chem, Urumqi 830017, Xinjiang, Peoples R China
2.Xinjiang Acad Agr Sci Sci, Inst Hort Crops, Sci Observing & Expt Stn Pomol Xinjiang, Minist Agr, Urumqi 830091, Xinjiang, Peoples R China
3.Inst Drug Control Xinjiang Uygur Autonomous Reg, Urumqi 830017, Peoples R China
4.Dalian Minzu Univ, Key Lab Biotechnol & Bioresources Utilizat, Dalian 116600, Peoples R China
关键词： Three-phase liquid -liquid extraction; Membrane separation; Carrier agent; Biogenic amines; Liquid chromatography -mass spectrometry
期刊名称：FOOD CHEMISTRY （ 影响因子：9.231； 五年影响因子：8.795 ）
ISSN： 0308-8146
年卷期： 2022 年 387 卷
页码：
收录情况： SCI
摘要： Analysis of biogenic amines (BAs) is of great importance due to their toxicity and usage as indicators of food freshness. In this study, membrane-assisted three-phase liquid-liquid extraction (MA-3pLLE) was proposed to integrate extraction and back-extraction into a single step using a specially designed U-shaped device. Parameters affecting the performance of the extraction method were optimized. Coupled with liquid chromatography-mass spectrometry, the method was successfully applied for the simultaneous determination of eight BAs without derivatization in apple juice, orange juice, red wine, soy sauce and milk granules, with satisfactory recoveries and RSDs. The calibration curve of the method was linear in the range of 1.00-100.00 ng/mL, with a correlation coefficient (r2) >= 0.9908. The limits of detection were in the range of 0.03-1.00 ng/mL. MA-3pLLE is efficient, reproducible, and green and has great potential for application in the one-step extraction of analytes from complex matrices.
- 相关文献
