文献类型: 外文期刊
作者: Yu, Pingzhong 1 ; Jia, Chunhong 2 ; Song, Wencheng 3 ; Liu, Fengmao 1 ;
作者机构: 1.China Agr Univ, Coll Sci, Beijing 100193, Peoples R China
2.Beijing Acad Agr & Forestry Sci, Inst Plant Protect & Environm Protect, Beijing 100097, Peoples R China
3.Minist Agr, Inst Control Agrochem, Beijing 100125, Peoples R China
关键词: Flutriafol;Wheat;Soil;Dissipation
期刊名称:BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY ( 影响因子:2.151; 五年影响因子:2.129 )
ISSN: 0007-4861
年卷期: 2012 年 89 卷 5 期
页码:
收录情况: SCI
摘要: The dissipation and residues of flutriafol in wheat and soil under field conditions in Beijing, Anhui and Shandong in China were determined based on high performance liquid chromatography. Flutriafol were extracted with acetonitrile and cleaned up by solid-phase extraction with florisil cartridges before UV detection. The limits of detection and quantification of flutriafol were 0.04 ng and 0.01 mg/kg for both wheat and soil samples, respectively. The mean recoveries ranged from 93.4% to 96.4%, with relative standard deviation between 3.8% and 6.8% at three spiked levels (0.01, 0.1, 1.0 mg/kg). Half-lives were 13.3, 9.9 and 13.6 days in soil, while 15.2, 10.8 and 9.2 days in wheat plant in Beijing, Anhui and Shandong, respectively. The terminal residues of flutriafol were below the maximum residue limit 0.02 mg/kg set by Japan in wheat when pre-harvest interval were 35 days.
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