您好,欢迎访问广东省农业科学院 机构知识库!

Headspace solid-phase microextraction-gas chromatography-mass spectrometry analysis of the volatile components of longan (Dimocarpus longan Lour.)

文献类型: 外文期刊

作者: Zhang, Yi 1 ; Gao, Bei 1 ; Zhang, Mingwei 1 ; Shi, John 3 ; Xu, Yujuan 2 ;

作者机构: 1.Huazhong Agr Univ, Coll Food Sci & Technol, Wuhan 430070, Peoples R China

2.Guangdong Acad Agr Sci, Agrobiotech Res Inst, Guangzhou 510610, Guangdong, Peoples R China

3.Agr & Agri Food Canada, Guleph Food Res Ctr, Guelph, ON N1G 5C9, Canada

关键词: Longan;HS-SPME;GC-MS;Volatile components;Optimization;Central composite design

期刊名称:EUROPEAN FOOD RESEARCH AND TECHNOLOGY ( 影响因子:2.998; 五年影响因子:3.005 )

ISSN: 1438-2377

年卷期: 2009 年 229 卷 3 期

页码:

收录情况: SCI

摘要: Headspace solid-phase microextraction has been applied to the analysis of volatile components in longan (Dimocarpus longan Lour.). Silica fiber coated with divinylbenzene-carboxen-polydimethylsiloxane (DVB-CAR-PDMS) was found to be more efficient for extracting volatile compounds than other fibers such as those coated with polydimethylsiloxane, polyacrylate, and carboxen-polydimethylsiloxane. The SPME headspace volatiles were collected using a DVB-CAR-PDMS fiber. The extraction conditions were optimized using a response surface experimental design to analyze the effect of three factors: extraction temperature, equilibrium time and extraction time. The best response was obtained when the extraction temperature was around 50 A degrees C, equilibrium time near 15 min and extraction time close to 25 min. The volatile extracts were analyzed using gas chromatograph/mass spectrometry system. Sixty-two different volatile compounds from the headspace of longan were identified. The linearity was good in the considered concentration ranges (R (2) a parts per thousand yen 0.965). Average recoveries ranged from 78.6 to 108.3% and showed good accuracy. The precision of the present method was found to be good (RSD < 13.59%). Therefore, this method can be applied to determine the quality of the longan or other volatile components as an alternative to full-scale headspace analysis.

  • 相关文献

[1]桑椹挥发性成分的GC-MS分析. 陈智毅,张友胜,徐玉娟,吴继军,李升锋,刘学铭. (Mis

[2]Recent Advances in Postharvest Research on Longan Fruit. Han, D. M.,Li, J. G.,Pan, X. W.,Li, R.,Guo, D. L.,Han, D. M.,Li, J. G.,Pan, X. W.,Li, R.,Guo, D. L.,Wu, Z. X.,Shuai, L.,Wu, Z. X.. 2014

[3]Physicochemical Characteristics and Immunomodulatory Activities of Three Polysaccharide-Protein Complexes of Longan Pulp. Yi, Yang,Liao, Sen Tai,Zhang, Ming Wei,Zhang, Rui Fen,Deng, Yuan Yuan,Wei, Zhen Cheng,Yi, Yang,Shi, John. 2011

[4]Effect of microwave power on kinetics and characteristics of microwave vacuum-dried longan (Dimocarpus longan Lour.) pulp. Su, Dongxiao,Zhang, Mingwei,Wei, Zhencheng,Tang, Xiaojun,Zhang, Ruifen,Liu, Lei,Deng, Yuanyuan,Su, Dongxiao,Zhang, Mingwei.

[5]Sucrose-metabolizing enzymes and their genes in the arils of two Dimocarpus longan cultivars. Shuai, L.,Li, J.,Niu, J. J.,Qian, P. H.,Liu, W. H.,Xue, X. Q.,Wu, Z. X.,Shuai, L.,Han, D. M.,Shuai, L.,Li, J.,Niu, J. J.,Qian, P. H.,Liu, W. H.,Xue, X. Q.,Wu, Z. X..

[6]Optimization of extraction conditions of total phenol from lotus (Nelumbo nuficera Gaertn) rhizome. Yang, Dong-Mei,Zhang, Qian,Wang, Hui-Li,Zhu, Xing-Yi,Wang, Qiu-Shuang,Ying, Tie-Jin. 2012

[7]Enhanced Mycelial Biomass Production of the Hairy Bracket Mushroom, Trametes hirsuta (Higher Basidiomycetes), by Optimizing Medium Component with Plackett-Burman Design and Response Surface Methodology. Yang, Rongling,Liu, Xueming,Zhao, Xiangjie,Xu, Yujuan,Ma, Rongxia,Zhao, Xiangjie.

[8]榆叶梅精油的提取及成分分析. 李,陈炳旭. 2011

[9]不同制备工艺柴胡注射液成分分析及质量标准探讨. 陈文露,彭新宇,余静贤,高彪,徐志宏,潘育方. 2019

[10]广佛手不同成熟期果实挥发性物质含量分析. 钟云,袁显,曾继吾,姜波,蒋侬辉. 2013

[11]橡木桶陈酿处理对沙田柚蒸馏酒挥发性风味成分的影响. 移兰丽,余元善,杜昌陈,徐玉娟,陈卫东,吴继军. 2016

[12]火焰花挥发性成分的SPME-GC/MS分析. 杨艳,杨春英,杨荣玲,刘学铭. 2014

[13]几种干燥方式对金针菇子实体挥发性风味成分的影响. 唐秋实,陈智毅,刘学铭,杨春英,王思远,林耀盛. 2015

[14]龙眼核乙酸乙酯萃取物的GC-MS分析. 黄儒强,刘学铭. 2005

[15]乌龙茶香气的HS-SPME-GC-MS/GC-O研究. 苗爱清,吕海鹏,孙世利,王力,庞式,赖兆祥,曾琼,林智. 2010

[16]不同季节翠玉品种茶叶香气组分的GC-MS分析. 赖幸菲,庞式,李裕南,徐平,潘顺顺. 2014

[17]广州输入性花卉蓟马的种类组成及种群动态分析. 陈婷,齐国君,高燕,吕利华. 2014

[18]岭头单枞乌龙茶HS-SPME/GC-MS/GC-O研究. 苗爱清,吕海鹏,孙世利,王力,庞式,赖兆祥,曾琼. 2010

[19]荔枝果汁饮料和荔枝原汁挥发性成分分析. 移兰丽,余元善,肖更生,徐玉娟,吴继军,邹波. 2016

[20]干燥条件对茶枝柑果皮黄酮和精油成分的影响. 周菲菲,肖更生,林羡,徐玉娟,吴继军,陈于陇,傅曼琴. 2015

作者其他论文 更多>>