Iodine-catalyzed synthesis of sulfonyl isoxazoles from sodium sulfinates and isoxazol-5(4H)-ones
文献类型： 外文期刊
第一作者： Tang, Dong
作者： Tang, Dong;Iqbal, Zafar;Sun, Jian;Ji, Jingwen;Yang, Zhixiang;Tang, Dong;Yang, Minghua
作者机构：
关键词： Sulfonyl isoxazole; Sodium sulfinate; Isoxazol-5(4H)-ones; Iodine-catalyzed; Organic sodium salt
期刊名称：TETRAHEDRON LETTERS （ 影响因子：2.415； 五年影响因子：2.036 ）
ISSN： 0040-4039
年卷期： 2021 年 62 卷
页码：
收录情况： SCI
摘要： An efficient I-2-mediated sulfonylation at 4-position of isoxazoles has been developed by employing sodium sulfinate and 3-substituted isoxazol-5(4H)-ones. This metal-free, one-pot strategy provides various sulfonyl isoxazoles under mild reaction conditions. The final product exists in the form of stable organic sodium salt, which can be purified by column chromatography under air. (C) 2020 Elsevier Ltd. All rights reserved.
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