Simultaneous Determination of 6 Neonicotinoid Residues in Soil Using DLLME-HPLC and UV

文献类型： 外文期刊

第一作者： Sun Bao-li

作者： Sun Bao-li;Shan Hong;Li Yan-hua;Zeng Ya-ling;Shen Xiu-li;Tong Cheng-feng

作者机构：

关键词： HPLC;UV;Dispersive liquid-liquid micro-extraction;Neonicotinoid;Soil

期刊名称：SPECTROSCOPY AND SPECTRAL ANALYSIS （ 影响因子：0.589； 五年影响因子：0.504 ）

ISSN： 1000-0593

年卷期： 2013 年 33 卷 9 期

页码：

收录情况： SCI

摘要： A simple, cheap and rugged method was developed for simultaneous deter mination of 6 neonicotinoid residues in soil, including imidacloprid, acetamiprid, thiamethoxam, thiacloprid, clothianidin and nitenpyram. The soil sample was produced by dispersive liquid-liquid micro-extraction (DLLME) after extracted by the mixed solution of acetonitrile and CH2Cl2 (2 1, phi). The analytes were separated by HPLC with Alltima (TM) C-18 column (4. 6 mmX 250 mm, 5 mu m) and detected by PDA at 260 tun. External standard method was used for quantification. The results showed that good linearity was obtained with correlation coefficients between 0. 998 2 and 0. 999 9 in the range of 0. 5 similar to 200 mu g.L-1. The limits of detection (LODs) were in the range between 0. 000 5 and 0. 003 mu g.mL(-1) (S/N=3). The method was validated with five soil samples spiked at three fortification levels (0. 05, 0. 1, 1.0 mg.kg(-1)) and recoveries were in the range of 55. 3%similar to 95. 6% with RSD of 1. 4%similar to 7. 0%. The effect of clean-up was evaluated by UV spectra and demonstrated that the method established is effective. In conclusion, this method is competent for the simultaneous analysis of 6 neonicotinoid residues in soil.

分类号：

  • 相关文献

[1]Enantioselective Degradation of Chiral Insecticide Dinotefuran in Greenhouse Cucumber and Soil. Dong, Fengshou,Xu, Jun,Liu, Xingang,Wang, Yunhao,Zheng, Yongquan,Chen, Xiu.

[2]High Performance Liquid Chromatography determination of Fentin Acetate Residue in Beet and Soil. Sun Hui-qing,Li Yi-qiang,Xu Guang-jun,Zheng Xiao,Xu Jin-li,Wang Xiu-guo. 2012

[3]Determination of twelve herbicides in tobacco by a combination of solid-liquid-solid dispersive extraction using multi-walled carbon nanotubes, dispersive liquid-liquid micro-extraction, and detection by GC with triple quadrupole mass spectrometry. Liao, Qie Gen,Zhou, Yao Min,Luo, Lin Guang,Wang, Li Bing,Feng, Xiao Hu.

[4]Biodegradation and chemical characteristics of hot-water extractable organic matter from soils under four different vegetation types in the Wuyi Mountains, southeastern China. Bu, Xiaoli,Ding, Jiumin,Wang, Limin,Huang, Wei,Ruan, Honghua,Bu, Xiaoli,Yu, Xingna,Ding, Jiumin,Wang, Limin. 2011

[5]Horizontal migration of Acartia pacifica Steuer (copepoda) in response to UV-radiation. Zengling, M. A.,Wei, L. I.,Kunshan, G. A. O.,Zengling, M. A..

[6]Cyclobutane pyrimidine dimers photolyase from extremophilic microalga: Remarkable UVB resistance and efficient DNA damage repair. Li, Chongjie,Wang, Yibin,Zheng, Zhou,Liu, Fangming,Qi, Xiaoqing,An, Meiling,Chen, Hao,Miao, Jinlai,Ma, Li,Ma, Li,Mou, Shanli,Miao, Jinlai.

[7]Behavioral responses of zooplankton to solar radiation changes: in situ evidence. Ma, Zengling,Li, Wei,Gao, Kunshan,Shen, Anglv.

[8]Quantitative evaluation and discrimination of wild Paris polyphylla var. yunnanensis (Franch.) Hand.-Mazz from three regions of Yunnan Province using UHPLC-UV-MS and UV spectroscopy couple with partial least squares discriminant analysis. Yang, Yuangui,Zhang, Jinyu,Wang, Yuanzhong,Yang, Yuangui,Jin, Hang,Zhang, Ji,Zhang, Jinyu,Wang, Yuanzhong,Yang, Yuangui,Jin, Hang,Zhang, Ji,Zhang, Jinyu,Wang, Yuanzhong.

[9]Lethal and sublethal effects of dinotefuran on two invasive whiteflies, Bemisia tabaci (Hemiptera: Aleyrodidae). Qu, Cheng,Zhang, Wei,Li, Fengqi,Luo, Chen,Wang, Ran,Tetreau, Guillaume. 2017

[10]Determination of neonicotinoid insecticides residues in eels using subcritical water extraction and ultra-performance liquid chromatography-tandem mass spectrometry. Xiao, Zhiming,Yang, Yunxia,Li, Yang,Fan, Xia,Ding, Shuangying.

[11]Individual and Joint Acute Toxicities of Selected Insecticides Against Bombyx mori (Lepidoptera: Bombycidae). Yu, R. X.,Wang, Y. H.,Hu, X. Q.,Wu, S. G.,Cai, L. M.,Zhao, X. P..

[12]Systemic action of novel neonicotinoid insecticide IPP-10 and its effect on the feeding behaviour of Rhopalosiphum padi on wheat. Cui, Li,Sun, Lina,Cao, Yazhong,Yang, Daibin,Yuan, Huizhu,Shao, Xusheng,Li, Zhong.

[13]Insecticide resistance in Bemisia tabaci biotype Q (Hemiptera: Aleyrodidae) from China. Luo, C.,Jones, C. M.,Devine, G.,Denholm, I.,Gorman, K.,Luo, C.,Zhang, F..

[14]Design, synthesis and insecticidal activity of novel hydrocarbylidene nitrohydrazinecarboximidamides. Yang, Dong-yan,Zhou, Zi-yuan,Ma, Yong-qiang,Qin, Zhao-hai,Zou, Xiang-gao,Rui, Chang-hui.

[15]Lethal and sublethal effects of thiamethoxam on the whitefly predator Serangium japonicum (Coleoptera: Coccinellidae) through different exposure routes. Yao, Feng-Luan,Zheng, Yu,Zhao, Jian-Wei,He, Yu-Xian,Weng, Qi-Yong,Desneux, Nicolas.

[16]Lethal, sublethal and transgenerational effects of the novel chiral neonicotinoid pesticide cycloxaprid on demographic and behavioral traits of Aphis gossypii (Hemiptera: Aphididae). Li, Jin-Hua,Liu, Yong-Qiang,Cui, Li,Lu, Yan-Hui,Wu, Kong-Ming,Yuan, Hai-Bin,Li, Jin-Hua,Xu, Xiao-Yong,Li, Zhong,Desneux, Nicolas. 2017

[17]Lethal effect of imidacloprid on the coccinellid predator Serangium japonicum and sublethal effects on predator voracity and on functional response to the whitefly Bemisia tabaci. Wu, Kongming,He, Yuxian,Zhao, Jianwei,Zheng, Yu,Desneux, Nicolas. 2012

[18]Susceptibility to neonicotinoids and risk of resistance development in the brown planthopper, Nilaparvata lugens (St(a)over-circlel) (Homoptera: Delphacidae). Zhu, Yu Cheng,Wang, Yanhua,Chen, Jin,Ma, Chongyong,Huang, Yue,Shen, Jinliang,Wang, Yanhua. 2008

[19]Does Drought Increase the Risk of Insects Developing Behavioral Resistance to Systemic Insecticides?. Khodaverdi, Haleh,Fowles, Trevor,Bick, Emily,Nansen, Christian,Nansen, Christian.

[20]Transcriptomic responses to different doses of cycloxaprid involved in detoxification and stress response in the whitebacked planthopper, Sogatella furcifera. Yang, Yuanxue,Zhang, Yixi,Yang, Baojun,Liu, Zewen,Fang, Jichao.

作者其他论文 更多>>

微信小程序