Determination of flavomycin residue in grass carp by high performance liquid chromatography

文献类型： 外文期刊

第一作者： Tian Liang-liang

作者： Tian Liang-liang;Huang Dong-mei;Shi Yong-fu;Han Feng;Zhou Peng

作者机构：

关键词： High performance liquid chromatography;grass carp;flavomycin;residues

期刊名称：PROCEEDINGS OF THE 3RD INTERNATIONAL CONFERENCE ON MATERIAL, MECHANICAL AND MANUFACTURING ENGINEERING

ISSN： 2352-5401

年卷期： 2015 年 27 卷

页码：

收录情况： SCI

摘要： A method for the determination of flavomycin in shrimp by high performance liquid chromatography was established. Flavomycin in sample was extracted by methanol solution and defatted with n-hexane. The lower was cleaned through the membrane and determined by HPLC. The calibration curve was linear. The method was accurate and reproducible, being successfully applied to the monitoring of flavomycin in grass carp. The recoveries were 83.9 %-88.2 % in the spiked range of 2.0-50.0 mg/kg in grass carp. The relative standard deviation was below 10.4%. The limit of detection for this method as defined by ten times signal to noise was 2.0mg/kg.

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