Determination of Abamectin Residues in Grain by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

文献类型： 外文期刊

第一作者： He Hong-Mei

作者： He Hong-Mei;Zhao Hua;Zhang Chun-Rong;Zhu Ya-Hong;Ping Li-Feng;Wu Min;Zhang Chang-Peng;Cai Xiao-Ming;Li Zhen

作者机构：

关键词： Abamectin residues;Ultra performance liquid chromatography-tandem mass spectrometry;Grain

期刊名称：CHINESE JOURNAL OF ANALYTICAL CHEMISTRY （ 影响因子：1.134； 五年影响因子：0.909 ）

ISSN： 0253-3820

年卷期： 2013 年 41 卷 11 期

页码：

收录情况： SCI

摘要： A new analytical method has been developed for the simultaneous determination of abamectin residues such as abamectin, ivermectin and emamectin benzoate in grain. The samples of brown rice, wheat and corn were extracted with acetonitrile by an oscillator, cleaned up by acid alumina column, and analyzed by gradient ultra performance liquid chromatography-tandem mass spectrometry with electrospray ionization in positive mode (ESI+) using a UPLC BEH C-18 Column. The method was validated using fortified brown rice, wheat and corn. Mean recoveries of grain at four spiked levels (10, 50, 100. 0 and 1000 mu g/kg) were found between 87% and 109% with good precision (RSD<8%) for brown rice, wheat and corn. Mean recovery of within-laboratory reproducibility was between 97% and 107% with good precision (RSD <9%) for all the pesticides at the spiked level of 50 mu g/kg. Limits of detection (LODs) for abamectin, ivermectin and emamectin benzoate in brown rice, wheat and corn were 0.5, 0.5 and 0.1 mu g/kg, which are lower than the maximum residue limit (MRL) established by Chinese, Japanese and European legislation in grain. Good linear relationships were obtained in the range of 2.0-64 mu g/L for abamectin and ivermectin, and in the range of 0.5-32 mu g/L for emamectin benzoate with the correlation coefficient over 0.997.

分类号：

  • 相关文献

[1]Identification of quantitative trait locus of zinc and phosphorus density in wheat (Triticum aestivum L.) grain. Shi, Rongli,Zhang, Fusuo,Zou, Chunqin,Li, Hongwei,Tong, Yiping,Jing, Ruilian.

[2]Simultaneous Determination of 14 Kinds of beta-Agonist Residues in Sheep Saliva by Ultra Performance Liquid Chramatogrephy-Tandem Mass Spectrometry. Li Yang,Su Xiao-Ou,Wang Rui-Guo,Wang Pei-Long,Zhang Wei,Chen Jie. 2013

[3]Simultaneous Determination of Plant Growth Regulators and Imidacloprid, Acetamiprid in Tea by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry. Zhu Li,Wang Chen,Chen Hong-Ping,Zhang Ying-Bin,Zhou Su-Juan,Wang Guo-Qing,Liu Xin. 2017

[4]Residue Analysis of SIOC0426 in Environmental Samples and Its Degradation in Soil. He Hong-Mei,Wu Min,Zhang Chun-Rong,Yu Jian-Zhong,Zhao Hua,Zhu Ya-Hong,He Kai-Yu,Zhang Chang-Peng,Cai Lei-Ming,Xu Ling-Ying,He Hong-Mei,Wu Min,Zhang Chun-Rong,Yu Jian-Zhong,Zhao Hua,Zhu Ya-Hong,He Kai-Yu,Zhang Chang-Peng,Cai Lei-Ming,Xu Ling-Ying,Tang Qing-Hong. 2017

[5]Determination of Glyphosate, Aminomethyl Phosphonic Acid and Glufosinate in Different Teas by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry. Zhu Li,Chen Hong-Ping,Zhou Su-Juan,Wang Chuan-Pi,Liu Xin. 2015

[6]Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry Analysis of 16 Kinds of Residual Antibiotics in Chicken Manure. Wu Dan,Zou De-Xun,Wu Dan,Han Mei-Lin,Wang Xu-Ming,Gao Min,Qiu Tian-Lei. 2017

[7]Residue and Degradation of Cyantraniliprole and Its Main Metabolite in Pepper and Soil. He Hong-Mei,Zhang Chun-Rong,Zhu Ya-Hong,Zhang Chang-Peng,Ping Li-Feng,Zhao Hua,Wu Min,Tang Tao,Cai Xiao-Ming,Li Zhen. 2014

[8]Simultaneous Determination of 3 Kinds of Isomers of Clorprenaline and Baclofen Residues in Feed by Ultra Performance Liquid Chromatography-Tandem Mass spectrometry. Li Yang,Su Xiao-Ou,Wang Pei-Long,Fan Xia,Wang Rui-Guo,Wang Xiao. 2014

[9]Dissipation, transfer and safety evaluation of emamectin benzoate in tea. Chen, Zongmao.

[10]Determination of Abamectin Residue in Paddy Rice by Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry. He Hong-Mei,Zhao Hua,Zhang Chun-Rong,Hu Xiu-Qing,Ping Li-Feng,Wu Min,Zhang Chang-Peng,Cai Xiao-Ming,Zhu Ya-Hong,Li Zhen. 2012

[11]Mineral element concentrations in grains of Chinese wheat cultivars. Yong Zhang,Qichao Song,Jun Yan,Jianwei Tang,Rongrong Zhao,Yueqiang Zhang,Zhonghu He,Chunqin Zou,Ivan Ortiz-Monasterio. 2010

[12]Multi-pesticides residue analysis of grains using modified magnetic nanoparticle adsorbent for facile and efficient cleanup. Liu, Zhenzhen,Qi, Peipei,Wang, Xiangyun,Wang, Zhiwei,Xu, Xiahong,Zhang, Hu,Wang, Qiang,Wang, Xinquan,Liu, Zhenzhen,Chen, Wenxue,Wang, Qiang,Qi, Peipei,Wang, Xiangyun,Wang, Qiang,Qi, Peipei,Wang, Xiangyun,Wang, Zhiwei,Xu, Xiahong,Zhang, Hu,Wang, Xinquan,Wang, Zhiwei,Xu, Xiahong,Zhang, Hu,Wang, Xinquan.

[13]Interspecific complementary and competitive interactions between intercropped maize and faba bean. Li, L,Yang, SC,Li, XL,Zhang, FS,Christie, P.

[14]Coupled Effects of Soil Water and Nutrients on Growth and Yields of Maize Plants in a Semi-Arid Region. Sun Zhan-Xiang,Zheng Jia-Ming,Sun Wen-Tao.

[15]Cultivar differences in photosynthetic tolerance to photooxidation and shading in rice (Oryza sativa L.). Jiao, DM,Li, X. 2001

[16]Characteristics and influencing factors of grass-feeding livestock breeding in China: An economic geographical perspective. Wang Guogang,Wang Mingli,Wang Jimin,Yang Chun,Liu Yufeng. 2016

[17]Arsenic Distribution, Species, and Its Effect on Maize Growth Treated with Arsenate. Ci Xiao-ke,Liu Hua-lin,Hao Yu-bo,Zhang Ji-wang,Liu Peng,Dong Shu-ting,Liu Hua-lin,Ci Xiao-ke. 2012

[18]Study on Near-Infrared Spectroscopy Signal Pre-processing and Model Building. Zhang Xiaochao,Zhang Yinqiao,Wang Hui. 2009

[19]Zinc biofortification of wheat through fertilizer applications in different locations of China. Zhang, Yue-Qiang,Karim, Md. Rezaul,Xue, Yan-Fang,Yan, Peng,Meng, Qing-Feng,Cui, Zhen-Ling,Zhang, Fu-Suo,Zou, Chun-Qin,Sun, Yi-Xiang,Ye, You-Liang,Cakmak, Ismail. 2012

[20]Cadmium and lead contamination in japonica rice grains and its variation among the different locations in southeast China. Cheng, FM,Zhao, NC,Xu, HM,Li, Y,Zhang, WF,Zhu, ZW,Chen, MX. 2006

作者其他论文 更多>>

微信小程序