Determination of imidacloprid,carbendazim and thiabendazole residues in vegetables and fruits by HPLC

文献类型： 外文期刊

第一作者： Lin, Ling

作者： Lin, Ling;Peng, Zheng;Yang, Chunliang;Wang, Mingyue;Zha, Yubing;Liu, Lili;Zeng, Shaodong

作者机构：

关键词： HPLC;fruits;Vegetables;imidacloprid;carbendazim;thiabendazole;residue

期刊名称：ADVANCES IN CHEMICAL ENGINEERING III, PTS 1-4

ISSN： 1022-6680

年卷期： 2013 年 781-784 卷

页码：

收录情况： SCI

摘要： The aim of this work was to establish a method that the residues of imidacloprid,carbendazim and thiabendazole in fruits and vegetables were determined by HPLC.Acetonitrile was edded in the sample for extraction solvent, and using sodium chloride for absorbing water of the sample,then purified by NH2 solid phase extraction cartridge, the sample was detected by HPLC.Under the selected conditions,the detection limits of imidacloprid, carbendazim, thiabendazole were 0.002 mg/kg,0.003 mg/kg and 0.003 mg/kg respectively,Tests for recovery were made by addition of three pesticides's standards at three different concentration levels(0.1, 0.5 and 1.0 mg/kg) to the blank sample.The mean recovery rates of imidacloprid, carbendazimand thiabendazole were 87.0%similar to 99.2%,82.0%similar to 96.0% and 80.0%similar to 95.0% respectively, and the relative standard deviations were 0.52%similar to 6.80%.The sensitivity, accuracy and precision of this method were able to meet the requirements for pesticide residue analysis.

分类号：

  • 相关文献

[1]Determination of ametoctradin residue in fruits and vegetables by modified quick, easy, cheap, effective, rugged, and safe method using ultra-performance liquid chromatography/tandem mass spectrometry. Liu, Xingang,Dong, Fengshou,Xu, Jun,Li, Shasha,Xu, Hanqing,Zheng, Yongquan. 2015

[2]Capillary Electrochromatography with Liquid Crystal Crown Ether Modified Hybrid Silica Monolith for Analysis of Imidacloprid and Carbendazim in Tomatoes. Wang, Mingming,Feng, Rui,Chen, Hao,Shen, Jing,Zeng, Zhaorui.

[3]Principles, developments and applications of computer vision for external quality inspection of fruits and vegetables: A review. Zhang, Baohua,Huang, Wenqian,Li, Jiangbo,Zhao, Chunjiang,Fan, Shuxiang,Wu, Jitao,Zhang, Baohua,Zhao, Chunjiang,Liu, Chengliang. 2014

[4]Determination of organochlorine pesticides in propolis by gas chromatography-electron capture detection using double column series solid-phase extraction. Chen, Fang,Chen, Lanzhen,Zhou, Jinhui,Xue, Xiaofeng,Zhao, Jing,Wang, Qiang.

[5]Monitoring, exposure and risk assessment of sulfur dioxide residues in fresh or dried fruits and vegetables in China. Lou, Tiantian,Huang, Weisu,Wu, Xiaodan,Wang, Mengmeng,Lu, Baiyi,Hu, Yinzhou,Huang, Weisu,Zhou, Liying,Zheng, Lufei.

[6]Simultaneous determination of pyrimethanil, cyprodinil, mepanipyrim and its metabolite in fresh and home-processed fruit and vegetables by a QuEChERS method coupled with UPLC-MS/MS. Liu, Xingang,Dong, Fengshou,Xu, Jun,Li, Yuanbo,Tian, Yingying,Zhang, Ying,Han, Yongtao,Zheng, Yongquan,Qin, Dongmei. 2013

[7]Residue analysis of four diacylhydrazine insecticides in fruits and vegetables by Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method using ultra-performance liquid chromatography coupled to tandem mass spectrometry. Liu, Xingang,Xu, Jun,Dong, Fengshou,Li, Yuanbo,Zheng, Yongquan,Song, Wenchen.

[8]A novel approach for simultaneous determination of E/Z-fluoxastrobins in vegetables and fruits by UHPLC-DAD. Sun, Qiang,Wang, Weimin,Li, Yubo,Wen, Guangyue,Tang, Hongxia,Song, Weiguo,Dong, Maofeng,Sun, Qiang,Tang, Hongxia.

[9]Simultaneous determination of organophosphorus pesticides in fruits and vegetables using atmospheric pressure gas chromatography quadrupole-time-of-flight mass spectrometry. Dong, Fengshou,Xu, Jun,Liu, Xingang,Wu, Xiaohu,Chen, Zenglong,Pan, Xinglu,Zheng, Yongquan,Dong, Fengshou,Gan, Jay.

[10]Chromatographic methods for the determination of pyrethrin and pyrethroid pesticide residues in crops, foods and environmental samples. Chen, ZM,Wang, YH. 1996

[11]Residues and dissipation kinetics of carbendazim and diethofencarb in tomato (Lycopersicon esculentum Mill.) and intake risk assessment. Li, Huidong,Du, Hongxia,Fang, Liping,Dong, Zhan,Guan, Shuai,Fan, Wenjing,Chen, Zilei,Li, Huidong,Du, Hongxia,Fang, Liping,Dong, Zhan,Guan, Shuai,Fan, Wenjing,Chen, Zilei.

[12]Influence of environmental factors on degradation of carbendazim by Bacillus pumilus strain NY97-1. Zhang, Lizhen,Qiao, Xiongwu,Ma, Liping,Zhang, Lizhen.

[13]Residue Analysis of Forchlorfenuron in Fruit and vegetable by RP-HPLC. Zhang, Hua,Yang, Xin,Dong, Ai Jun,Ma, Ying,Wang, Zhen Yu,Yang, Lin,Zhang, Ying Chun,Yang, Xin,Wang, Jing. 2010

[14]Dissipation dynamics of fenamidone and propamocarb hydrochloride in pepper, soil and residue analysis in vegetables by ultra-performance liquid chromatography coupled with tandem mass spectrometry. Li, Shasha,Hu, Mingfeng,Xu, Jun,Wu, Xiaohu,Dong, Fengshou,Zheng, Yongquan,Liu, Xingang.

[15]Determination of diflubenzuron residues in vegetables by UPLC-MS/MS. Wang, Xiaofang,Yang, Chunliang,Huang, Maofang,Wang, Mingyue,Zha, Yubing,Lin, Ling,Zeng, Shaodong. 2014

[16]Residue behavior and risk assessment of mixed formulation of imidacloprid and chlorfenapyr in chieh-qua under field conditions. Huang, Jian Xiang,Liu, Cong Yun,Lu, Da Hai,Chen, Jia Jia,Deng, Yi Cai,Wang, Fu Hua,Huang, Jian Xiang,Liu, Cong Yun,Lu, Da Hai,Chen, Jia Jia,Deng, Yi Cai,Wang, Fu Hua,Huang, Jian Xiang,Liu, Cong Yun,Lu, Da Hai,Chen, Jia Jia,Deng, Yi Cai,Wang, Fu Hua.

[17]Effect of pesticide 1-[6-chloro-3-methyl-pyridyl-8-nitro-7-methyl-1 2 3 5 6 7-hexahydro imidazo (1,2a)]-pyridine when responding to a wheat plant's antioxidant defense system. Wang, P.,Yang, X.,Huang, W. W.,Zhang, M.,Lu, W. H.,Zhao, H. T.,Dong, A. J.,Zhang, H.,Xu, R. B.,Zou, P.,Cheng, C. L.,Zhang, Y. C.,Jing, J.,Wang, P.,Yang, X.,Wang, J.,Wang, P..

[18]Degradation Dynamics of Glyphosate in Different Types of Citrus Orchard Soils in China. Zhang, Changpeng,Hu, Xiuqing,Luo, Jinyan,Wu, Zhiyi,Wang, Li,Li, Bin,Wang, Yanli,Sun, Guochang.

[19]Simultaneous Determination of Abietic Acid and Dehydroabietic Acid Residues in Duck Meat by HPLC-PAD-FLD. Zhu, Yongzhi,Zhang, Suzhen,Geng, Zhiming,Wang, Daoying,Liu, Fang,Zhang, Muhan,Bian, Huan,Xu, Weimin,Zhang, Suzhen.

[20]Synthesis and biological activity of novel benzimidazole derivatives as potential antifungal agents. Zhang, Tao,She, Dongmei,Ning, Jun,Mei, Xiangdong,Li, Yaofa,Pan, Wenliang,Gao, Zhanlin.

作者其他论文 更多>>

微信小程序