Volatolomics approach for authentication of not-from-concentrate (NFC) orange juice based on characteristic volatile markers using headspace solid phase microextraction (HS-SPME) combined with GC-MS

文献类型: 外文期刊

第一作者: Zhang, Jiukai

作者: Zhang, Jiukai;Sun, Ruixue;Xing, Ranran;Yu, Ning;Deng, Tingting;Ni, Xue;Chen, Ying;Liu, Hanlu;Zhao, Yan

作者机构:

关键词: Not-from-concentrate (NFC) juice; Volatolomics; Authentication; GC-MS; Chemometrics

期刊名称:FOOD CONTROL ( 影响因子:6.652; 五年影响因子:6.498 )

ISSN: 0956-7135

年卷期: 2022 年 136 卷

页码:

收录情况: SCI

摘要: The not-from-concentrate (NFC) juice is gradually becoming popular with consumers. However, adulteration of NFC juice with low-priced from-concentrate (FC) juice has been a long-lasting concern. In the present study, a volatolomics approach for authentication of NFC orange juice based on volatile organic compounds (VOCs) was established. A total of 107 VOCs were identified by solid phase microextraction (SPME) GC-Q-Exactive Orbitrap. Discrimination of NFC and FC orange juice could be accomplished by orthogonal partial least squares discrim-inant analysis (OPLS-DA). Furthermore, 10 VOCs were selected as potential characteristic markers in different juices, including 4 esters, 5 alcohols and 1 ketone. In addition, 13 VOCs with significant quantitative difference was also screened. A partial least squares discriminant analysis (PLS-DA) model based on the above 23 VOCs achieved accuracy of 100% and 95.6% for calibration and prediction set, respectively. These results suggested that the volatolomics approach has great potential for authentication of NFC juice.

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