Qualitative and Quantitative Determination of Decoquinate in Chicken Tissues by Gas Chromatography Tandem Mass Spectrometry
文献类型： 外文期刊
作者： Liu, Shuyu 1 ; Tang, Yayun 1 ; Lu, Yang 1 ; Guo, Yawen 1 ; Xie, Kaizhou 1 ; Guan, Fanxun 1 ; Gao, Pengfei 1 ; Zhu, Yali 1 ; Dong, Yuhao 3 ; Zhang, Tao 1 ; Zhang, Genxi 1 ; Dai, Guojun 1 ; Xie, Xing 4 ;
作者机构： 1.Yangzhou Univ, Coll Anim Sci & Technol, Yangzhou 225009, Peoples R China
2.Yangzhou Univ, Joint Int Res Lab Agr & Agriprod Safety, Yangzhou 225009, Peoples R China
3.Nanjing Agr Univ, Coll Vet Med, Nanjing 210095, Peoples R China
4.Jiangsu Acad Agr Sci, Inst Vet Med, Key Lab Vet Biol Engn & Technol, Minist Agr, Nanjing 210014, Peoples R China
关键词： decoquinate; gc-ms/ms; derivatization; chicken tissues; acetic anhydride
期刊名称：MOLECULES （ 影响因子：4.6； 五年影响因子：4.9 ）
ISSN：
年卷期： 2023 年 28 卷 9 期
页码：
收录情况： SCI
摘要： A novel precolumn derivatization-GC-MS/MS method was developed for the determination of decoquinate residues in chicken tissues (muscle, liver, and kidney). The samples were extracted and purified by liquid-liquid extraction combined with solid-phase extraction and derivatized with acetic anhydride and pyridine. The recovery rates for decoquinate were 77.38 similar to 89.65%, and the intra-day and inter-day RSDs were 1.63 similar to 5.74% and 2.27 similar to 8.06%, respectively. The technique parameters meet the necessities for veterinary drug residue detection in China, the US, and the EU. Finally, the method was applied to analyze tissues of 60 chickens bought from a neighborhood supermarket, and solely one sample of chicken muscle contained 15.6 mu g/kg decoquinate residue.
- 相关文献
作者其他论文 更多>>
-
Combining GC-MS/MS with a LLE-SPE sample pretreatment step to simultaneously analyse enrofloxacin and ofloxacin residues in chicken tissues and pork
作者：Pang, Maoda;Wang, Ran;Xu, Junjie;Tang, Yayun;Guo, Yawen;Ding, Hao;Zhang, Tao;Zhang, Genxi;Guo, Xiaodong;Dai, Guojun;Xie, Kaizhou;Xie, Xing;Xie, Xing
关键词：Chicken tissues; Pork; Enrofloxacin; Ofloxacin; GC-MS/MS
-
Development of a QuEChERS-HPLC-FLD Procedure for the Simultaneous Detection of Residues of Florfenicol, Its Metabolite Florfenicol Amine, and Three Fluoroquinolones in Eggs
作者：Guo, Yawen;Hong, Lu;Liu, Shuyu;Zhu, Yali;Zhang, Genxi;Xie, Kaizhou;Guo, Yawen;Hong, Lu;Liu, Shuyu;Zhu, Yali;Zhang, Genxi;Xie, Kaizhou;Gao, Pengfei;Gao, Pengfei;Xie, Xing
关键词：florfenicol; fluoroquinolones; HPLC-FLD; QuEChERS; egg
-
Determination of Tilmicosin in Poultry and Pork Meat by a Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) Preparation Method and Gas Chromatography-Tandem Mass Spectrometry (GC-MS/MS)
作者：Guo, Yawen;Liu, Shuyu;Tang, Yayun;Zhu, Yali;Xie, Kaizhou;Guo, Yawen;Liu, Shuyu;Tang, Yayun;Zhu, Yali;Xie, Kaizhou;Xie, Xing;Xie, Xing
关键词：Food safety; gas chromatography-tandem mass spectrometry (GC-MS/MS); poultry and pork meat; QuEChERS; tilmicosin
-
A rapid solid-phase extraction purification combined with UPLC-MS/MS used for simultaneous determination of eight tetracyclines and three metabolite in chicken and pork
作者：Gao, Pengfei;Chen, Lan;Ding, Hao;Xie, Kaizhou;Gao, Pengfei;Xie, Xing;Gao, Pengfei;Guo, Yawen;Chen, Lan;Ding, Hao;Xu, Junjie;Liu, Shuyu;Zhu, Yali;Zhang, Tao;Xie, Kaizhou;Guo, Yawen;Xu, Junjie;Liu, Shuyu;Zhu, Yali;Zhang, Tao;Xie, Kaizhou;Xie, Xing
关键词：Tetracycline antibiotics; Chicken; Pork; Residues; UPLC-MS/MS
-
A novel HPLC-PDA method for judging chicken meat infected with Salmonella Enteritidis by simultaneous determination of four key
作者：Xu, Junjie;Cao, Yang;Hong, Yiwei;Guo, Yawen;Hong, Lu;Cai, Jingjing;Cheng, Sihui;Guo, Xiaodong;Zhang, Tao;Zhang, Genxi;Xie, Kaizhou;Xu, Junjie;Ding, Hao;Chen, Lan;Cao, Yang;Hong, Yiwei;Guo, Yawen;Gao, Pengfei;Hong, Lu;Cai, Jingjing;Cheng, Sihui;Guo, Xiaodong;Zhang, Tao;Zhang, Genxi;Xie, Kaizhou;Ding, Hao;Chen, Lan;Gao, Pengfei;Pang, Maoda
关键词：Chicken meat; Salmonella Enteritidis; Metabolite biomarkers; HPLC-PDA; L-proline; L-valine; L-methionine; L-leucine
-
Pre-column derivatization with trimethylsilyl diazomethane coupled with ASE-SPE-GC-MS/MS method for the quantification and validation of penicillin G residues in poultry tissues and pork
作者：Liu, Chujun;Guo, Yawen;Xie, Kaizhou;Bao, Wenbin;Xie, Xing;Feng, Zhixin;Wang, Bo;Dong, Yuhao;Yang, Chenggen;Xie, Kaizhou
关键词：Penicillin G; TMSD; ASE; Poultry tissues; Pork; GC-MS; MS; Food analysis; Food composition
-
Effects of konjac glucomannan on physical properties and microstructure of fish myofibrillar protein gel: Phase behaviours involved
作者：Zhang, Tao;Zhuang, Xinbo;Chen, Yinji;Chen, Shengjun;Xu, Xiaoqi;Xue, Yong;Xue, Changhu;Jiang, Ning
关键词：Phase behavior; Dynamic rheology; Myofibrillar protein; Konjac glucomannan; Blended system
