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Bio-derived solvent-based automated dispersive liquid-liquid microextraction for pretreatment of diamide insecticides in environmental water samples

文献类型： 外文期刊

作者： Liu, Jin 1 ; Wang, Yuxin 1 ; Song, Rui 2 ; Yang, Yukun 3 ; Li, Li 2 ; Jing, Xu 1 ;

作者机构： 1.Shanxi Agr Univ, Coll Food Sci & Engn, Taigu 030801, Shanxi, Peoples R China

2.Shanxi Agr Univ, Coll Plant Protect, Shanxi Key Lab Integrated Pest Management Agr, Taiyuan 030031, Shanxi, Peoples R China

3.Shanxi Univ, Coll Life Sci, Taiyuan 030006, Shanxi, Peoples R China

期刊名称：GREEN CHEMISTRY （ 影响因子：9.2； 五年影响因子：9.8 ）

ISSN： 1463-9262

年卷期： 2024 年 27 卷 2 期

页码：

收录情况： SCI

摘要： A green, efficient, and cost-effective bio-derived solvent-based automated dispersive liquid-liquid microextraction (BDS-ADLLME) method was developed in the present study. A liquid handling platform with only the pipetting function module was employed to achieve automated multiple-sample pretreatment and eliminate manual errors. Green bio-derived solvents, gamma-valerolactone and eucalyptol, derived from renewable resources and exhibiting high environmental friendliness, were used as dispersant and extractant, respectively. The eucalyptol self-separated from the samples within 5 minutes, eliminating the need for centrifuges and demulsifiers. Four greenness evaluation tools confirmed that the BDS-ADLLME was an environmentally friendly sample pretreatment method meeting the requirements of green chemistry. The linear range was 0.006-3 mu g L-1 with R-2 > 0.999. The limit of detection was 0.002 mu g L-1. The BDS-ADLLME method successfully detected chlorantraniliprole and flubendiamide in tap, river, lake, and spring water samples, with recoveries and relative standard deviations ranging from 83.4-107.7% and 1.7%-5.4%, respectively. The BDS-ADLLME provides a feasible approach for developing automated eco-friendly dispersive liquid-liquid microextraction methods.

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