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Supercritical fluid CO2 extraction, simultaneous determination of components in ultra-fine powder of Ganoderma sinense by HPLC-ESI-MS method

文献类型： 外文期刊

作者： Chen, Ti-qiang 2 ; Zhao, Xiao-yan 3 ; Wu, Jin-zhong 1 ; Yu, De-yi 2 ; Wu, Yan-bing 1 ;

作者机构： 1.Fujian Coll TCM, Dept Pharmacol, Fuzhou 350013, Peoples R China

2.Fujian Acad Agr Sci, Fuzhou 350013, Peoples R China

3.Shandong Acad Agr Sci, Inst Agrofood Sci & Technol, Jinan 250100, Peoples R China

关键词： Ganoderma sinense; Ultra-fine powder of fruit-bodies; Chemical component; SFE; HPLC-ESI-MS

期刊名称：JOURNAL OF THE TAIWAN INSTITUTE OF CHEMICAL ENGINEERS （ 影响因子：5.876； 五年影响因子：5.294 ）

ISSN： 1876-1070

年卷期： 2011 年 42 卷 3 期

页码：

收录情况： SCI

摘要： An off-line mode coupled supercritical fluid extraction (SFE) with high-performance liquid chromatography and electro-spray ion trap mass spectrometry (HPLC-ESI-MS) analytical method was applied to analyze the chemical components of Ganoderma sinense (G. sinense). The ultra-fine powder of fruit-bodies of G. sinense was extracted by SFE and a HPLC-ESI-MS method was established for simultaneously determining chemical components of G. sinense, and the total extraction yield was 3.75% (w/w). The method of combining diode-array detection (DAD) with MS, was successfully used to detect the chemical components of G. sinense. Most of the peaks exhibited maximum absorptions at 280 and 210 nm, especially at 280 nm. About 20 peaks were acquired in positive and negative ion detection mode, and were analyzed by electro-spray ion trap mass spectrometry (ESI-ITMS). The results indicated that the molecular weight distribution (m/z: 188-614) of main compounds was identified according to the molecular ions in MS spectra. (C) 2010 Taiwan Institute of Chemical Engineers. Published by Elsevier B.V. All rights reserved.

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