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Determination of five Alternaria toxins in wolfberry using modified QuEChERS and ultra-high performance liquid chromatography-tandem mass spectrometry

文献类型： 外文期刊

作者： Xing, Lijie 1 ; Zou, Liangjun 1 ; Luo, Ruifeng 1 ; Wang, Yuan 1 ;

作者机构： 1.Xinjiang Acad Agr & Reclamat Sci, Anal & Testing Ctr, Shihezi 832000, Peoples R China

2.Xinjiang Prod & Construct Corps Inst Food Inspect, Shihezi 832000, Peoples R China

3.Lab Qual & Safety Risk Assessment Agroprod Shihez, Shihezi 832000, Peoples R China

4.Shihezi Univ, Sch Food Sci, Shihezi 832000, Peoples R China

关键词： Alternaria toxins; Modified QuEChERS; Ultra-high performance liquid; chromatography-tandem mass spectrometry; Wolfberry

期刊名称：FOOD CHEMISTRY （ 影响因子：7.514； 五年影响因子：7.516 ）

ISSN： 0308-8146

年卷期： 2020 年 311 卷

页码：

收录情况： SCI

摘要： A modified quick, easy, cheap, effective, rugged, and safe method coupled with ultra-high performance liquid chromatography-tandem mass spectrometry was established for the simultaneous detection of five Alternaria toxins (tenuazonic acid, alternariol, alternariol monomethyl ether, altenuene, and tentoxin) in wolfberry. The sample pretreatment conditions including the dilution solvent, the extraction solvent and the QuEChERS purification parameters were optimized. Detection of the five Alternaria toxins was performed in MRM mode under ESI + conditions. The results showed that the five Alternaria toxins exhibited good linearity (1-200 mu g/L, with correlation coefficients > 0.999). The limits of detection were 0.07-0.24 mu g/kg, and the limits of quantification were 0.32-0.77 mu g/kg. The trueness was between 73.8% and 111.5%, and the precision was lower than 10%. The established method was effectively used for the determination of five Alternaria toxins in 155 wolfberry samples from Northwest China.

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