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Development and Application of a QuEChERS-Based Liquid Chromatography Tandem Mass Spectrometry Method to Quantitate Multi-Component Alternaria Toxins in Jujube

文献类型： 外文期刊

作者： Wang, Cheng 1 ; Fan, Yingying 3 ; He, Weizhong 3 ; Hu, Dongqiang 5 ; Wu, Aibo; Wu, Wenliang 1 ;

作者机构： 1.China Agr Univ, Coll Resources & Environm Sci, Beijing Key Lab Biodivers & Organ Farming, Beijing 100193, Peoples R China

2.Xinjiang Acad Agr Sci, Management Sci Res, Urumqi 830091, Peoples R China

3.Minist Agr & Rural Affairs, Lab Qual & Safety Risk Assessment Agro Prod Urumq, Key Lab Agro Prod Qual & Safety Xinjiang, Urumqi 830091, Peoples R China

4.Xinjiang Acad Agr Sci, Inst Qual Stand & Testing Technol Agro Prod, Urumqi 830091, Peoples R China

5.Univ Chinese Acad Sci, Shanghai Inst Nutr &

关键词： Alternaria toxins; jujube; QuEChERS; UPLC-MS/MS

期刊名称：TOXINS （ 影响因子：4.546； 五年影响因子：4.8 ）

ISSN： 2072-6651

年卷期： 2018 年 10 卷 10 期

页码：

收录情况： SCI

摘要： A simple, rapid and efficient methodology was developed and validated for the analysis of four Alternaria toxins in jujube: Tenuazonic acid, alternariol, alternariol monomethyl ether, and tentoxin. Under the optimized extraction procedure, chromatographic conditions, and instrumental parameters, the four toxins were effectively extracted via a quick, easy, cheap, effective, rugged, and safe (QuEChERS) method, and quantified by ultra-performance liquid chromatography coupled to tandem mass spectrometry (UPLC-MS/MS). Matrix-matched calibrations ranging from 0.01 to 0.5 mu g mL(-1) were conducted for the quantification due to the matrix effect. A blank jujube sample was spiked at 40, 80 and 160 mu g kg(-1), obtaining recoveries in the range of 83.5-109.6%. Limits of detection and limits of quantification were in the range of 0.14-0.26 and 0.47-0.87 mu g kg(-1), respectively. Finally, the developed method was applied for the quantification of the four toxins in 14 jujube samples, including black spot-infected and uninfected samples. Results showed that the predominant toxin detected in all the samples was tenuazonic acid, the content of which was associated with the infection level; alternariol, alternariol monomethyl ether, and tentoxin were detected in all the infected samples and some of the uninfected samples with rather low contents.

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