Determination of the Carbamate Pesticides Fuberidazole and Pirimicarb in Crayfish (Procambarus Clarkii) Using Excitation-Emission Fluorescence Matrices with Self-Weighted Alternating Trilinear Decomposition (SWATLD)
文献类型： 外文期刊
作者： Liu, Yan 1 ; Wang, Chao 1 ; Xia, Zhenzhen 4 ; Wang, Qiao 1 ; Liu, Xin 1 ; Gong, Zhiyong 1 ;
作者机构： 1.Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan, Peoples R China
2.Wuhan Polytech Univ, Minist Educ, Coll Food Sci & Engn, Key Lab Deep Proc Major Grain & Oil, Wuhan, Peoples R China
3.Wuhan Polytech Univ, Coll Food Sci & Engn, Hubei Key Lab Proc & Transformat Agr Prod, Wuhan, Peoples R China
4.Hubei Acad Agr Sci, Inst Agr Qual Stand & Testing Technol Res, Wuhan, Peoples R China
5.Wuhan Polytech Univ, Coll Food Sci & Engn, Wuhan 430023, Peoples R China
关键词： Crayfish; excitation-emission fluorescence; fuberidazole; pirimicarb; self-weighted alternating trilinear decomposition (SWATLD); >
期刊名称：ANALYTICAL LETTERS （ 影响因子：2.0； 五年影响因子：1.8 ）
ISSN： 0003-2719
年卷期： 2023 年
页码：
收录情况： SCI
摘要： Fuberidazole and pirimicarb are carbamate pesticides for insect control. There is pesticide accumulation through the food chain that may ultimately migrate into the human body through the crayfish. Here a rapid method for simultaneous determination of fuberidazole and pirimicarb in crayfish is reported. The excitation-emission fluorescence matrix was obtained by simple pretreatment of crayfish meat using acetonitrile, and qualitative and quantitative information was separated from overlapping spectra using the self-weighted alternating trilinear decomposition. The detection limits of the pesticides for fuberidazole and pirimicarb were 0.068 mg/kg and 0.160 mg/kg, respectively, and the limits of quantitation were 0.207 mg/kg and 0.485 mg/kg. The average recoveries were 90.79% and 98.77%. The results show that a combination of excitation-emission fluorescence matrix and alternating trilinear decomposition can be used for the determination of fuberidazole and pirimicarb in crayfish with simple pretreatment using acetonitrile.
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