A rapid solid-phase extraction purification combined with UPLC-MS/MS used for simultaneous determination of eight tetracyclines and three metabolite in chicken and pork
文献类型： 外文期刊
作者： Gao, Pengfei 1 ; Guo, Yawen 3 ; Chen, Lan 1 ; Ding, Hao 1 ; Xu, Junjie 3 ; Liu, Shuyu 3 ; Zhu, Yali 3 ; Zhang, Tao 3 ; Xie, Xing 2 ; Xie, Kaizhou 1 ;
作者机构： 1.Yangzhou Univ, Coll Vet Med, Yangzhou 225009, Peoples R China
2.Jiangsu Acad Agr Sci, Inst Vet Med, Nanjing 210014, Peoples R China
3.Yangzhou Univ, Joint Int Res Lab Agr & Agriprod Safety, Yangzhou 225009, Peoples R China
4.Yangzhou Univ, Coll Anim Sci & Technol, Yangzhou 225009, Peoples R China
5.Minist Agr, Key Lab Vet Biol Engn & Technol, Nanjing 210014, Peoples R China
关键词： Tetracycline antibiotics; Chicken; Pork; Residues; UPLC-MS/MS
期刊名称：JOURNAL OF FOOD COMPOSITION AND ANALYSIS （ 影响因子：4.3； 五年影响因子：4.6 ）
ISSN： 0889-1575
年卷期： 2024 年 132 卷
页码：
收录情况： SCI
摘要： A method for rapid detection and identification of 8 tetracyclines (TCs) and 3 metabolite residues in chicken and pork was established and verified by combining rapid solid-phase extraction (SPE) technology with ultrahighperformance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). After a sample was extracted, it was purified with a PRiME HLB cartridge, and the cartridge did not need to be activated, balanced, or eluted. The filtrate was dried under nitrogen, redissolved, and subsequently analyzed via UPLC-MS/MS. The limits of detection for chicken and pork were 0.05-0.48 mu g/kg and 0.05-0.52 mu g/kg, respectively. The limits of quantification were 0.16-1.61 mu g/kg and 0.16-1.75 mu g/kg, respectively. The recoveries were 85.15%-107.50% and 84.21%-106.37%, respectively. The established method was suitable for qualitative and quantitative analyses of TCs and their metabolite residues in chicken and pork and has been used for the detection of TC in chicken and pork samples from local markets.
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