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A New Ni(II) Coordination Polymer Constructed by the Dicarboxylate and Imidazole-Containing Ligand With Three-Fold Interpenetrating pcu Topological Net: Synthesis, Crystal Structure, and Luminescent Property

文献类型： 外文期刊

作者： Xu, Jiakun 1 ; Sun, Xiaochun 3 ; Ju, Caixia 1 ; Zhang, Quan 1 ; Sun, Mi 1 ;

作者机构： 1.Chinese Acad Fishery Sci, Yellow Sea Fisheries Res Inst, Key Lab Sustainable Dev Marine Fisheries, Minist Agr, Qingdao 266071, Peoples R China

2.Ocean Univ China, Key Lab Marine Chem Theory & Technol, Minist Educ, Qingdao, Peoples R China

3.Natl Oceanog Ctr, Qingdao, Peoples R China

4.Shanghai Ocean Univ, Coll Food Sci & Technol, Shanghai, Peoples R China

关键词： coordination polymer;crystal structure;nickel (II)

期刊名称：SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY （ 影响因子：0.784； 五年影响因子：0.677 ）

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收录情况： SCI

摘要： A new Ni(II) coordination polymer with 2,4'-biphenyl-dicarboxylate acid (H_2bpdc) and 1,4-bis(4-pyridylmethy) piperazine (bpp) has been prepared by hydrothermal synthesis and characterized by single-crystal X-ray diffraction, IR, and EA. Complex [Ni(bpdc)2(bpp)_(1.5) (H_2O)]n(1), is triclinic system space group P-1 with a = 11.975(2) ?, b = 12.449(3) ?, c = 13.154(3) ?, α = 101.971(5)?, β = 111.961(4)?, γ = 91.211(3)?, V = 1768.6(12) ?~3, Z = 2, M_r = 716.75, D_c = 1.345g/cm~3, F(000) = 750, and μ = 0.60 cm~(-1). The final refinement gave R = 0.0594 and wR = 0.1587 for 6185 reflections with I > 2σ(I). X-ray diffraction analysis reveals that the title complex [Ni(bpdc)_2(bpp)_(1.5)(H_2O)]_n(1) displays a three-fold diamond topological net. Furthermore, the luminescent property of complex 1 is investigated.

  • 相关文献

[1]Construction of cadmium(II) and zinc(II) coordination frameworks based on 3,5-bis(benzoimidazo-1-ly)pyridine and carboxylate acids: Synthesis, crystal structures and photoluminescent properties. Xu, Jiakun,Wang, Shuaiyu,Sun, Mi,Xu, Jiakun,Yan, Xingchen,Sun, Xiaochun,Yan, Xingchen. 2013

[2]Synthesis, Crystal Structures and Luminescent Properties of pH-Dependent Zn (II) Coordination Polymers. Xu, Jiakun,Sun, Mi,Xu, Jiakun,Fan, Yuhua,Bi, Caifeng,Sun, Xiaochun. 2012

[3]Hydrothermal synthesis of five new coordination polymers based on benzophenone-2, 4'-dicarboxylic acid and N-donor spacers. Xu, Jiakun,Fan, Yuhua,Bi, Caifeng,Xu, Jiakun,Sun, Mi,Sun, Xiaochun.

[4]Crystal structures and theoretical calculations of two peculiar compounds derived from 4-benzoyl-3-methyl-1-phenyl-2-pyrazolin-5-one. Yan, Xingchen,Wu, Xiaojing,Xu, Jiakun,Fan, Yuhua,Bi, Caifeng,Zhang, Xia,Zhang, Zhongyu,Yan, Xingchen,Xu, Jiakun. 2014

[5]Zinc coordination polymers with rigid dicarboxylates and semirigid 3,5-bis(imidazole-1-yl) pyridine: syntheses, structural topologies, and luminescent properties. Xu, Jiakun,Ju, Caixia,Sheng, Jun,Wang, Fang,Sun, Mi,Sun, Xiaochun,Ju, Caixia.

[6]Crystal structure of 2-aminobenzothiazolinium nitrate and theoretical study of the amino-imino tautomerism of 2-aminobenzothiazole. Yan, Xingchen,Wu, Xiaojing,Xu, Jiakun,Fan, Yuhua,Bi, Caifeng,Zhang, Xia,Zhang, Zhongyu,Yan, Xingchen,Xu, Jiakun.

[7]Crystal structure of cyclic nucleotide-binding-like protein from Brucella abortus. He, Zheng,Gao, Yuan,Li, Xuemei,Zhang, Xuejun C.,He, Zheng,Dong, Jing,Ke, Yuehua,Chen, Zeliang.

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