Determination of Methylene Blue and Its Metabolite Residues in Aquatic Products by High-Performance Liquid Chromatography-Tandem Mass Spectrometry
文献类型： 外文期刊
作者： Zhang, Xuan 1 ; Hui, Yunhua 1 ; Fang, Changling 1 ; Wang, Yuan 1 ; Han, Feng 1 ; Lou, Xiaoyi 1 ; Fodjo, Essy Kouadio 3 ;
作者机构： 1.Chinese Acad Fishery Sci, East China Sea Fisheries Res Inst, Shanghai 200090, Peoples R China
2.Chinese Acad Fishery Sci, Key Lab East China, Sea Fisheries Res Inst, Shanghai 200090, Peoples R China
3.Univ Felix Houphouet Boigny, Phys Chem Lab, UFR SSMT, 22 BP 582, Abidjan, Cote Ivoire
关键词： high-performance liquid chromatography-tandem mass spectrometry; methylene blue; disinfectant; aquatic products
期刊名称：MOLECULES （ 影响因子：4.412； 五年影响因子：4.588 ）
ISSN：
年卷期： 2021 年 26 卷 16 期
页码：
收录情况： SCI
摘要： A sensitive and reliable method was developed to determine methylene blue (MB) and its metabolite residues, including azure A (AZA), azure B (AZB), and azure C (AZC) in aquatic products by HPLC-MS/MS. The samples were extracted by acetonitrile and cleaned up by alumina-neutral (ALN) cartridges. The analytes were separated on a Sunfire C18 column (150 mm x 2.1 mm, 5 mu m). The method was validated according to the European criteria of Commission Decision 2002/657/CE. Good linearity between 1-500 mu g/L was obtained with correlation coefficients (R-2) greater than 0.99. The limit of quantification (LOQ) was 1.0 mu g/kg. The average recoveries at three levels of each compound (1, 5, and 10 mu g/kg) were demonstrated to be in the range of 71.8-97.5%, with relative standard deviations (RSDs) from 1.05% to 8.63%. This method was suitable for the detection of methylene blue and its metabolite residues in aquatic products.
- 相关文献
作者其他论文 更多>>
-
One step cleanup of 160 pesticides and veterinary drugs in aquatic products using melamine-based automatic pressure filtration purification method combined with HPLC-MS/MS
作者：Zhou, Ruidong;Kong, Cong;Yang, Guangxin;Huang, Dongmei;Zhou, Ruidong;Wen, Yupeng;Huo, Wendi;Zhang, Chaoying;Sun, Huiwu;Liu, Huan;Li, Jincheng;Zhou, Ruidong;Wen, Yupeng;Huo, Wendi;Zhang, Chaoying;Sun, Huiwu;Liu, Huan;Li, Jincheng;Zhou, Ruidong;Wen, Yupeng;Huo, Wendi
关键词：Aquatic products; Pressure filtration cleanup column; Melamine sponge sorbent; Pesticides and veterinary drugs; Quantitative analysis; Health risk assessment
-
Simultaneous Determination of Seven Pyrethroid Pesticide Residues in Aquatic Products by Gas Chromatography
作者：Fang, Changling;Lou, Xiaoyi;Zhang, Xuan;Li, Siman;Tang, Yunyu;Shi, Yongfu;Huang, Dongmei
关键词：pyrethroids; aquatic products; gas chromatography; modified SPE pretreatment method; easy application
-
Rapid and selective detection of tetracyclic antibiotics in environmental water using Cu2+-doped hydrophilic imprinted melamine resin
作者：Gu, Lin;Ding, Shuhai;Zhang, Junyu;Yang, Guangxin;Ding, Shuhai;Zhang, Junyu;Yang, Guangxin;Wang, Longlong;Shen, Xiaoshen;Tian, Liangliang;Kong, Cong
关键词：Hydrophilic molecularly imprinted resin; Multiple adsorption mechanisms; Environmental samples; Tetracycline antibiotics
-
Survey of the biogenic amines in typical foods commonly consumed from the Chinese market
作者：Zhang, Xuan;Fang, Changling;Lou, Xiaoyi;Han, Feng;Li, Siman;Shi, Yongfu;Huang, Dongmei
关键词：Biogenic amines; Fish; Cheese; Alcoholic beverage; Risk assessment
-
Development and validation of rapid screening of 192 veterinary drug residues in aquatic products using HPLC-HRMS coupled with QuEChERS
作者：Yang, Guangxin;Zhang, Junyu;Tang, Yunyu;Kong, Cong;Li, Siman;Wang, Shouying;Ding, Shuhai;Shen, Xiaosheng;Chi, Hai;Yang, Guangxin;Zhang, Junyu;Ding, Shuhai;Gu, Lin;Martin, Aka Alla
关键词：High resolution mass spectrometry; QuEChERS; Veterinary drug; Aquatic products; Screening
-
Determination of Free Glycidol and Total Free Monochloropropanediol in Fish and Krill Oil with Simple Aqueous Derivatization and High-Performance Liquid Chromatography-Tandem Mass Spectrometry
作者：Yang, Guangxin;Tang, Yunyu;Liu, Xiaoxia;Wang, Longlong;Shen, Xiaosheng;Kong, Cong;Fan, Chengqi;Liu, Xiaoxia;Wang, Longlong;Qin, Lixia;Li, Dan;Zhai, Wenlei;Fodjo, Essy Kouadio
关键词：monochloropropanediol; glycidol; p-(dimethylamino)phenol; krill oil; fish oil; demulsification
-
A high-quality chromosome-level genome assembly of the topmouth culter (Culter alburnus Basilewsky, 1855)
作者：Zhao, Huali;Fang, Di-an;Xu, Dongpo;Fang, Di-an;Wang, Yuan;Zhang, Minying;Wang, Anqi;Xu, Yuanfeng;Xu, Dongpo
关键词：
