Multi-component screening coupled with ultrasound-assisted green extraction based on HPLC-HRMS for bio-actives analysis in saffron (Crocus sativus L.)
文献类型： 外文期刊
作者： Wang, Shouying 1 ; Song, Yiqing 1 ; Chen, Miaomiao 2 ; Bai, Bing 1 ; Zhou, Lin 3 ; Zhou, Changyan 1 ; Zhang, Yongchun 3 ; Huang, Zhiying 1 ; Si, Wenshuai 1 ;
作者机构： 1.Shanghai Acad Agr Sci, Inst Agrifood Stand & Testing Technol, Shanghai 201403, Peoples R China
2.Shanghai Univ Technol, Sch Hlth Sci & Engn, Shanghai 200093, Peoples R China
3.Shanghai Acad Agr Sci, Forest & Fruit Tree Res Inst, Shanghai 201403, Peoples R China
关键词： Crocus sativus L.; bioactive components; HPLC-HRMS; multivariate statistical analysis; antioxidant
期刊名称：FOOD CHEMISTRY-X （ 影响因子：8.2； 五年影响因子：8.2 ）
ISSN： 2590-1575
年卷期： 2025 年 25 卷
页码：
收录情况： SCI
摘要： A database of 115 bio-actives from seven subclasses, including information on retention time, parent ion m/z, fragment m/z, and isotopic fit, was established, and an instrumental method for simultaneous analysis of these targets was optimised. An ultrasound-assisted preparation method at 50 degrees C for 50 min with a 1:60 solid-liquid ratio, water as the solvent was proposed for the screening of unknown components and the antioxidant analysis in saffron. The self-built database and untargeted analysis identified 32 and 103 bio-actives in saffron, respectively. The comparative analysis revealed that the antioxidant capacity of saffron petals was superior to that of stigmas. Correlation and multivariate statistical analyses indicated that terpenoids may be the main active substances in stigmas, while flavonoids and carboxylic acid derivatives play a pivotal role in conferring antioxidant activity to de-stigmatised saffron. The method serves as an ideal tool for mining the functional components of saffron and other agricultural products.
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