Development of a vortex oscillating clean-up column for high-throughput semi-automatic sample preparation of drug residues in fish muscle tissues
文献类型： 外文期刊
作者： Zhou, Ruidong 1 ; Mu, Shuhe 1 ; Feng, Tengwang 1 ; Liu, Huan 1 ; Sun, Huiwu 1 ; Li, Jincheng 1 ;
作者机构： 1.Chinese Acad Fishery Sci, Beijing 100414, Peoples R China
2.Minist Agr, Key Lab Control Qual & Safety Aquat Prod, Beijing 100141, Peoples R China
3.Shanghai Ocean Univ, Coll Fisheries & Life Sci, Shanghai 201306, Peoples R China
关键词： Semi-automatic sample preparation; QuEChERS; HPLC-QTRAP-MS/MS; Vortex oscillating clean-up column; Food composition
期刊名称：JOURNAL OF FOOD COMPOSITION AND ANALYSIS （ 影响因子：4.52； 五年影响因子：4.942 ）
ISSN： 0889-1575
年卷期： 2022 年 109 卷
页码：
收录情况： SCI
摘要： A novelty high-throughput semi-automatic sample clean-up method was developed and used for rapid analysis of 9 drug residues in fish muscle tissues combined with high-performance liquid chromatography/quadrupolelinear ion trap mass spectrometry (HPLC-QTRAP-MS/MS). The target compounds were extracted by Quick, Easy, Cheap, Effective, Rugged and Safe multiresidue (QuEChERS) method with acetonitrile. A vortex oscillating clean-up column was proposed for single step purification firstly. After centrifugation, 1 mL of acetonitrile layer was transferred into a 3 mL vortex oscillating clean-up column which packed with 150 mg C-18 sorbent. The column was covered with piston, placed on a column-tube rack, vigorously agitated on a multi-tube vortex mixer. After vortex oscillation, purified extract was obtained for analysis by pushing the piston of oscillating clean-up column. The performance of the developed method was validated by analyzing 9 analytes in spiked grass carp muscle tissues. The limits of quantification (LOQs) ranged from 1.0 to 5.0 mu g kg( -1). The recoveries were in the range of 101-119% at the four concentration levels (2.0, 5.0, 10.0, 20.0 mu g kg( -1)). Inter-day and intra-day relative standard deviations (RSDs) were lower than 16% for all analytes.
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