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Preparation and evaluation of a novel chlorine dioxide preservative based on citric acid grafted carboxymethyl chitosan

文献类型： 外文期刊

作者： Wu, Guang 1 ; Zhou, Chuang 4 ; Yang, Ziming 4 ; Yin, Qingchun 5 ; Guo, Li 1 ; Deng, Hao 1 ;

作者机构： 1.Hainan Acad Agr Sci, Inst Agroprod Proc & Design, Key Lab Trop Fruit & Vegetable Cold chain Hainan P, Haikou 571100, Peoples R China

2.Hainan Acad Agr Sci, Sanya Inst, Sanya 572025, Peoples R China

3.Minist Agr & Rural Affairs, Key Lab Genet Resources Evaluat & Utilizat Trop Fr, Coconstruct Minist Prov, Haikou 571100, Peoples R China

4.China Acad Trop Agr Sci, South Subtrop Crop Res Inst, Key Lab Hainan Prov Postharvest Physiol & Preserva, Zhanjiang 524091, Peoples R China

5.Hainan Inst Food Control, Key Lab Trop Fruits & Vegetables Qual Safety State, Haikou 570314, Peoples R China

6.Hainan Acad Agr Sci, Agroprod Proc & Design, Haikou 571100, Hainan, Peoples R China

关键词： Carboxymethyl chitosan; ClO2 preservative; Longan; Preparation; Evaluation

期刊名称：INTERNATIONAL JOURNAL OF BIOLOGICAL MACROMOLECULES （ 影响因子：8.2； 五年影响因子：7.8 ）

ISSN： 0141-8130

年卷期： 2023 年 242 卷

页码：

收录情况： SCI

摘要： Instrument-free chlorine dioxide (ClO2) preservative for fruit and vegetable has gained great attention due to its convenience and safety. In this study, a series of carboxymethyl chitosan (CMC) with citric acid (CA) substituents were synthesized, characterized, and further used to prepare a novel ClO2 slow-releasing preservative for longan. UV-Vis and FT-IR spectra revealed that CMC-CA#1-3 were successfully prepared. Further potentiometric titration showed that the mass ratios of CA grafted in CMC-CA#1-3 were 0.18:1, 0.42:1, and 0.42:1, respectively. The composition and concentration of ClO2 slow-releasing preservative were optimized, and the best formulation was as follows: NaClO2:CMC-CA#2:Na2SO4:starch = 3:2:1:1. The maximum ClO2 release time of this preservative reached >240 h at 5-25 degrees C, and the maximum release rate always occurred at 12-36 h. Longan treated with 0.15-1.2 g ClO2 preservative had significantly (p < 0.05) higher L* and a* values but lower respiration rate and total microbial colony counts than the CK group (0 g ClO2 preservative). After 17 days of storage, longan treated with 0.3 g ClO2 preservative had the highest L* value of 47.47 and lowest respiration rate of 34.42 mg.kg(-1).h(-1), showing the best pericarp color and pulp quality. This study provided a safe, effective, and simple solution for longan preservation.

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