您好，欢迎访问浙江省农业科学院 机构知识库！
浙江省农业科学院机构知识库

全部

  • 全部
  • 标题
  • 学者
  • 机构
  • 关键词

Development of rapid low temperature assistant modified QuEChERS method for simultaneous determination of 107 pesticides and relevant metabolites in animal lipid

文献类型： 外文期刊

作者： Zhao, Huiyu 1 ; Zhao, Zhenni 2 ; Li, Xue 1 ; Di, Shanshan 1 ; Qi, Peipei 1 ; Wang, Zhiwei 2 ; Wang, Jiao 2 ; Tian, Pei 2 ; Xu, Hao 2 ; Wang, Xinquan 1 ;

作者机构： 1.Zhejiang Acad Agr Sci, Inst Agroprod Safety & Nutr, State Key Lab Managing Biot & Chem Threats Qual &, Key Lab Detect Pesticide Residues & Control Zhejia, Hangzhou 310021, Peoples R China

2.Agr Minist Key Lab Pesticide Residue Detect, Hangzhou 310021, Peoples R China

3.Desheng Middle Rd 298, Hangzhou 310021, Zhejiang, Peoples R China

关键词： Pesticides; QuEChERS; LC-MS/MS; Muti-residue; Animal lipid; High fat matrix

期刊名称：FOOD CHEMISTRY （ 影响因子：9.231； 五年影响因子：8.795 ）

ISSN： 0308-8146

年卷期： 2022 年 395 卷

页码：

收录情况： SCI

摘要： A modified QuEChERS LC-MS/MS method was developed for 107 pesticides analysis in animal lipids such as pork lard, mutton tallow, chicken oil and butter. The challenges for high fat matrices clean up were studied in details by optimizing dispersive purification adsorbents coupled with rapid low temperature assistant methods. The method validation was carried out using pork lard and further appplied to other matrices by testing their recoveries. Good linearities were obtained with correlation coefficients greater than 0.99. Sensitive LOQs ranged from 5.0-50.0 mu g kg(-1). Both inter-day and intra-day precisions were lower than 20% indicating the good precision and accuracy of this method. The method applied to four animal lipids with 93%similar to 100% of analytes revealed satisfactory recoveries (ranged from 70% to 120%) and RSD (<= 20%) at 10 mu g kg(-1) and 50 mu g kg(-1) spiking levels respectively related to the matrix.

  • 相关文献
作者其他论文 更多>>
置顶
购物车
反馈

© 京ICP备09089781号-29 主办单位：浙江省农业科学院

学术资源： 中国农业科学院 农业专业知识服务系统 农科联盟资源共建共享平台 中国农业科技文献与信息服务平台 中国农业期刊集成服务平台