Ionic liquid-based ultrasonic/microwave-assisted extraction combined with UPLC-MS-MS for the determination of tannins in Galla chinensis
文献类型: 外文期刊
作者: Lu, Chunxia 1 ; Wang, Hongxin 1 ; Lv, Wenping 1 ; Ma, Chaoyang 1 ; Lou, Zaixiang 1 ; Xie, Jun 2 ; Liu, Bo 2 ;
作者机构: 1.Jiangnan Univ, Sch Food Sci & Technol, State Key Lab Food Sci & Technol, Wuxi 214122, Peoples R China
2.Chinese Acad Fishery Sci, Freshwater Fisheries Res Ctr, Key Open Lab Genet Breeding Aquat Anim & Aquacult, Minist Agr, Wuxi 214081, Peoples R China
关键词: Galla chinensis;ionic liquid;tannins;ultrasonic/microwave-assisted extraction;UPLC-MS/MS
期刊名称:NATURAL PRODUCT RESEARCH ( 影响因子:2.861; 五年影响因子:2.572 )
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收录情况: SCI
摘要: Ionic liquid was used as extraction solvents and applied to the extraction of tannins from Galla chinensis in the simultaneous ultrasonic- and microwave-assisted extraction (UMAE) technique. Several parameters of UMAE were optimised, and the results were compared with of the conventional extraction techniques. Under optimal conditions, the content of tannins was 630.2±12.1mgg 1. Compared with the conventional heat-reflux extraction, maceration extraction, regular ultrasound- and microwave-assisted extraction, the proposed approach exhibited higher efficiency (11.7-22.0% enhanced) and shorter extraction time (from 6h to 1min). The tannins were then identified by ultraperformance liquid chromatography tandem mass spectrometry. This study suggests that ionic liquid-based UMAE is an efficient, rapid, simple and green sample preparation technique.
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