Optimization of the ultrasound-assisted synthesis of lutein disuccinate using uniform design
文献类型： 外文期刊
作者： Li, Da-Jing 1 ; Song, Jiang-Feng 1 ; Xu, Ai-Qin 2 ; Liu, Chun-Quan 1 ;
作者机构： 1.Jiangsu Acad Agr Sci, Inst Farm Prod Proc, Nanjing 210014, Jiangsu, Peoples R China
2.Nanjing Agr Univ, Coll Food Sci & Technol, Nanjing 210095, Jiangsu, Peoples R China
3.Northeast Forestry Univ, Coll Forestry, Harbin 150040, Peoples R China
关键词： LC-MS analysis;Lutein disuccinate;NMR spectroscopy;Ultrasound-assisted synthesis;Uniform design
期刊名称：ULTRASONICS SONOCHEMISTRY （ 影响因子：7.491； 五年影响因子：7.537 ）
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年卷期：
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收录情况： SCI
摘要： The ultrasound-assisted synthesis of lutein disuccinate from all-trans lutein (AL) and succinic anhydride (SA) was investigated in this study. Triethylamine was used as the catalyst. Based on the single-factor experiments, a 7-level-3-factor uniform design and response surface analysis were further employed to evaluate the effects of the selected variables including molar ratio of SA/AL, reaction time and ultrasonic power on the yield of lutein disuccinate. The results indicated that the data were adequately fitted into a second-order polynomial model; the molar ratio of SA/AL significantly affected the synthesis of lutein disuccinate, whereas reaction time and ultrasonic power did not. Based on ridge max analysis, the optimum condition for lutein disuccinate synthesis was predicted to be the molar ratio of SA/AL 265.3:1, ultrasonic power 300 W and reaction time 131.6 min with the lutein disuccinate yield of 80.53 ± 0.18%, which give a 43.8% increase compared with the traditional method, and also significantly shorten the reaction time.
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