Sensitive Determination of Bioactive Crocin Analogues in Gardenia Jasminoides Ellis using SPE prior to HPLC Analysis
文献类型： 外文期刊
作者： Zhang, Xiaoling 1 ; Yu, Huijuan 1 ;
作者机构： 1.Chinese Acad Fishery Sci, East China Sea Fisheries Res Inst, Key Lab East China Sea & Ocean Fishery Resources, Minist Agr China, Shanghai 200090, Peoples R China
关键词： Single-walled carbon nanotubes;SPE;Crocin analogues;Gardenia Jasminoides Ellis
期刊名称：SENSORS, MEASUREMENT AND INTELLIGENT MATERIALS, PTS 1-4
ISSN： 1660-9336
年卷期： 2013 年 303-306 卷
页码：
收录情况： SCI
摘要： In this study, the feasibility of single-walled carbon nanotubes (SWCNTs) as solid-phase extraction (SPE) adsorbent for the determination of bioactive crocin analogues in the traditional Chinese Medicine (TCM) of Gardenia Jasminoides Ellis prior to HPLC analysis was studied. Various experimental factors influencing SPE efficiency and HPLC conditions were studied. By using SWCNTs as the SPE adsorbent, the detection limit of 1.19-2.21 fmol (at S/N of 3) were achieved with the preconcentration efficiency of more than 120-folds, indicating this proposed method was very practical for increasing the sensitivity prior to HPLC analysis, and it may provides useful clue for the efficient extraction for the bioactive compounds in TCMs.
- 相关文献
作者其他论文 更多>>
-
Taxonomic, Phylogenomic and Bioactivity Profiling of Novel Phycosphere Bacterium from Model Cyanobacterium Synechococcus elongatus PCC 7942
作者：Zhang, Xiaoling;Xu, Jiaquan;Zhang, Xiaoling;Dai, Jun;Zhang, Xiaoling;Yang, Qiao;Xu, Jiaquan;Zhang, Lei;Feng, Lijuan;Yang, Qiao;Xu, Jiaquan;Yang, Qiao;Tian, Xiaoqing;Yang, Qiao
关键词：phycosphere microbiota; algae-bacteria interactions; marine model cyanobacterium; bioactive exopolysaccharides; microalgae growth-promoting bacterium; CO2 fixation efficiency by microalgae; Synechococcus elongatus PCC 7942
-
Multi-Residue Screening of Pesticides in Aquatic Products Using High-Performance Liquid Chromatography-Tandem High-Resolution Mass Spectrometry
作者：Wang, Shouying;Yang, Guangxin;Tang, Yunyu;Wang, Yuan;Shen, Xiaosheng;Yu, Huijuan;Kong, Cong;Wang, Shouying;Si, Wenshuai;Zhai, Wenlei;Fodjo, Essy Kouadio
关键词：pesticide residues; multi-residue screening; aquatic product; high-resolution mass spectrometry; sample preparation; QuEChERS; fish; crab; crayfish
-
Implications for practical application of commercial reduced iron powders to activate aqueous sulfite for decontamination of organics
作者：Lou, Xiaoyi;Fang, Changling;Yu, Huijuan;Guo, Yaoguang;Guan, Jie;Guo, Yaoguang;Zhou, Tianyi;Zhu, Xuefeng
关键词：Sulfate radicals; Advanced oxidation processes; Decontamination; Radical quenching
-
Simultaneous determination of ten aminoglycoside antibiotics in aquatic feeds by high-performance liquid chromatography quadrupole-orbitrap mass spectrometry with pass-through cleanup
作者：Lou, Xiaoyi;Tang, Yunyu;Fang, Changling;Kong, Cong;Yu, Huijuan;Shi, Yongfu;Huang, Dongmei;Xiao, Dongxue;Lou, Xiaoyi;Tang, Yunyu;Fang, Changling;Kong, Cong;Yu, Huijuan;Shi, Yongfu;Huang, Dongmei;Guo, Yaoguang;Guo, Yaoguang;Xiao, Dongxue
关键词：antibiotic residues; exploration of detection method; instrumental analysis; modified solid phase extraction; optimization
-
Multiclass screening of > 200 pharmaceutical and other residues in aquatic foods by ultrahigh-performance liquid chromatography-quadrupole-Orbitrap mass spectrometry
作者：Kong, Cong;Wang, Yang;Huang, Yuanfei;Wang, Yang;Huang, Yuanfei;Yu, Huijuan
关键词：Veterinary drug; Aquatic food; Screening; Orbitrap; Pesticide; Contaminant residue
-
Ponticoccus alexandrii sp nov., a novel bacterium isolated from the marine toxigenic dinoflagellate Alexandrium minutum
作者：Yang, Qiao;Zhang, Xiaoling;Feng, Lijuan;Mu, Jun;Li, Lingzhi;Zhang, Ruonan
关键词：Ponticoccus alexandrii sp nov; Marine dinoflagellate; Alexandrium minutum; Algal-associated bacterium
-
Screening Assay Establishment for Toxigenic Bacteria from PSP-producing Dinoflagellate Alexandrium tamarense Cultures
作者：Zhang, Xiaoling
关键词：PSP toxins;Alexandrium tamarense;Toxigenic bacteria;Screening Assay
